HAFeCrAl纤维生物功能梯度材料的制备及其性能.pdfVIP

中南大学学报(自然科学版) 而1.42 No.6 第42 卷第6 期 2011 年6 月 Journal ofCentral South University (Science and Technology) June 2011 HA/FeCrAl 纤维生物功能梯度材料的制备及其性能 童晓阳，邹俭鹏，阮建明，杨海林，节云峰 (中南大学粉末冶金国家重点实验室，湖南长沙， 410083) 摘要t 采用热压技术制备HAlFeCrAl纤维功能梯度材料(FGM)，并借助 SEM， EDAX 和双D 等对HAlFeCrAl 纤维FGM 的性能和微观结构进行测试及观察。研究结果表明: HAlFeCrAI 纤维FGM 按 FeCrAl 纤维体积含量呈 2.5%-5.0%一7.5%一10.0%-15.0%-20.0%梯度变化，梯度层之间模糊过渡。梯度层内纤维分布均匀，无明显的 孔洞或裂纹等缺陆存在，两相界面融合良好。经稀盐酸预处理后，纤维表面产生的凹陆有利于纤维与基体紧密结 合。HA/FeCrAl 纤维 FGM 整体抗弯强度为 78.89 MPa，体现出较明显的纤维拔出增强机制及层间裂纹偏转增韧机 制。HAlFeCrAl纤维 FGM 的物相为 HA 和 FeCrAl，无其他杂质相出现，无任何两相间及与热压模具间的反应 发生. 关键词z 费基磷灰石; FeCrAl纤维:功能梯度材料:热压:微观结构 中固分类号z τB333 文献标志码:A 文章编号: 1672-7207(2011)06- 1567-06 Preparation and properties of HAlFeCrAl fibers biological functional gradient materials TONG Xiao-yang, ZOU Jian-peng , RUAN Jian-mi吨， YANGHai-l尬，且E Yun-feng (State Key Laboratory ofPowder Metallurgy, Central South Universi纱， Changsha 41ω83， China) Abstrad: HAlFeCrAl fiber FGM w挝fabricated with hot pressing technique . SEM, EDAX and XRD were carried outω characterize i凶 perfonnance and microstructure. The results show 也刻也ere are gradient changes in the FGM with FeCrAl fiber contents changing as 2.5%-5.00fo一7.5%一10.~也一15.0%-20.0% and there is indistinct transition between gradient layers. Bo也HA and FeCrAl 缸e evenly distributed in 也e gradient layers and interface 缸sion of the two 庐ases is excellent. No obvious pores or cracks appear in the FGM. A负er pre位eatment of diluted hydrochloric acid, the depression in fiber surface let fiber and m且往ix integrate better. Comprehensive bending s位ength of FGM is 78.89 MPa. There exist FeCrAl fiber pull-out