应用毛细管气相色谱技术测定化妆品中防腐剂苯甲醇含量.pdfVIP

应用毛细管气相色谱技术测定化妆品中防腐剂苯甲醇含量份 r 缸瞿堕 作者简介 1.上海市质最监督检验执术研究院/罔家食品质量监督检验 中心(上海) ，上海 200233; 周耀斌，男，高级技师，从事食品安 2. 上海出入境检验检疫局，上海 200123 全与化妆品检测研究。 电话:021; 周耀斌1 彭亚锋1 雷 涛1 产罗是2 Email: zhouyb777向hotmail. com þ. ι ，巳，曾、_. e霞1 采用越声抽提法对化妆品中的苯甲醇进行了气相色谱测定的研究，建立了…种简单、快速、准确测定化妆品中苯甲醇的 测定方法。结果表明，该方法能够有效地提取化妆品中的苯用自事.并可对旦进行测定。苯甲醇加标凶收率为 99.08%-104.47% (n 1 日，相对标准偏浆。.971 %-3.53% (n = 15) ，检出限为 0.005% • 组盟h 气相ß谱化妆品苯甲醇 Determination of Benzyl Alcohol in Cosmetics by Gas Chromatography 梯 ZHOU Yaobin l PENG Yafeng 1 LEI Tao 1 YAN Luomei 2 (1. Shanghai Institute of Quality Inspection and Technical Research/ National Food Quality Supervision and Inspection Center (Shanghai) , Shanghai 200233 , China; 2. Shanghai Entry-Exit Inspection And Quarantine Bureau , Shanghai 200123 , China ) Abstract Gas chromatography has been used to analyze benzyl alcohol in cosmetics. 丁he results indicated that ultrasonic ex- traction and gas chromatography have been used to analyze benzyl alcohol in cosmetics effectively. A simple. rapid and accurate method for the determination of benzyl alcohol in cosmetics has been established. The results showed that the method could ef- fectively extract and determine benzyl alcohol in cosmetics. The mean recovery rate for cosmetic sample are 99.08% -104.47 % (n = 1 日， the standard deviations are O. 971 % -3. 53 % (n = 15) •and the limit of detection was O. 005 %. Key words gas chromatography cosmetics benzyl alcohol 苯甲醇又称节醇(benzyl alcohol) ，是一种芳香