亲水性C18硅胶反相色谱柱同时分离测定红茶中的有机酸.PDF

5 8 Vol. 5 No. 8 2014 8 Journal of Food Safety and Quality Aug. , 2014 C18 1 1 1,2* 1 1,2 1 张 静 , 蒋华军 , 刘仲华 , 陈金华 , 林 勇 , 邹文敏 (1. , 410128; 2. , 410128) 摘 要: 目的 C18 11 方法 ACCHROM XAqua C 18 (4.6 mm150 mm, 5 μm), 0.1% -, 1.0 mL/min, 25 ℃, 214 nm 结果 11 13 min , 92.07%~101.64%, 0.54%~1.93%, r 0.9986 6 , (668.62 mg/L), (386.67 mg/L); , 119.67~193.18 mg/L; (0~193.43 mg/L)(36.62~193.98 mg/L) 结论 , , 关键词: C18 ; ; Simultaneous separation and determination of organic acids in black tea by high performance liquid chromatography using polar-enhanced C18 column 1 1 1,2* ZHANG Jing , JIANG Hua-Jun , LIU Zhong-Hua , CHEN Jin-Hua, LIN Yong1,2, ZOU Wen-Min1 (1. Key Laboratory of Ministry of Education for Tea Science, Hunan Agricultural University , Changsha 410128, China; 2. National Research Center of Engineering Technology for Utilization of Botanical Functional Ingredients, Changsha 410128, China) ABSTRACT: Objective To establish a method for the simultaneous separation and determination o