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纯银分析方法
11 纯银分析 1
11.1 氯化银沉淀-原子吸收补正法测定银(Determination of Silver by Atomic Absorption Spectrometry after Precipitation with Silver Chloride) 1
11.2 原子吸收光谱法测定铁、铅和铋(Determination of Iron, Lead and Bismuth by Atomic Absorption Spectrometry) 2
11.3 原子吸收光谱法测定金和铜(Determination of Gold and Copper by Atomic Absorption Spectrometry) 2
11.4 5-Br-PADAP吸光光度法测定锑(Determination of Antimony by 2-(5-Bromo-2-pyridylazo)-5–Diethylaminophenol Spectrophotometry) 3
11.5 燃烧-电导法测定碳(Determination of Carbon by Combustion-Conductometric Method) 4
11.6 燃烧-碘酸钾滴定法测定硫(Determination of Sulphur by Combustion-potassium Iodate Titration) 6
11.7 ICP-AES法测定杂质元素(Determination of Impurity Elements by ICP-AES ) 8
11.8金属棒状原子发射光谱法测定杂质元素〔Determination of Impurity Elements Metal by Metal Rod Shape Spectrographic Method〕 8
11.9 双硫腙吸光光度法测定铅(Determination of Lead by Dithizone Spectrophotometry) 9
11.10 火焰原子吸收光谱法测定镁和锌(Determination of Magnesium and Zine by Flame Atomic Absorption Spectrometry) 11
11.11 火焰原子吸收光谱法测定镉(Determination of Cadmium by Flame Atomic Absorption Spectrometry) 12
11.12 孔雀绿吸光光度法测定锑(Determination of Antimony by Melachite Green Spectrophtometry) 12
11.13 邻菲罗啉吸光光度法测定铁(Determination of Iron by 1,10 Phenanthroline Spectrophotometry) 14
11.14 马钱子碱-碘化钾吸光光度法测定铋(Determination of Bismuth by Brucine- Iodide Spectrophotometry) 14
11.15 磷钼蓝吸光光度法测定磷(Determination of Phosphorus by ArsenicmolybdenumBlue Spectrophotometry) 15
11.16 化学光谱测定铅、铋、锌等15种杂质元素(Determination of Impurity Elements by Chemical Spectrographic Method ) 16
11.17 直读光谱法测定金、铜、铁等11种杂质元素(Determination of Impurity Elements by Direct-reading Spectrometry Method) 19
11.18 电感耦合等离子质谱法测定铜、锌、硒等9种杂质元素(Determination of Impurity Elements by Inductively Coupled Plasma-Mass Spectrometry Method ) 20
参考文献 21
11 纯银分析
11.1 氯化银沉淀-原子吸收补正法测定银(Determination of Silver by Atomic Absorption Spectrometrrecipitation with Silver Chloride)
nm处,使用空气-乙炔火焰测量银的吸光度。
本法适用于99.90%~99.99%银含量的测定。
仪器及试剂
原子吸收光谱仪:配备空气-乙炔火焰燃烧器及银空心阴极灯。
振荡机:250次/min;试银瓶:200mL磨口瓶。
银标准溶液(1.00mg/mL):称取1.0000g银(质量分
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