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huaxue（huaxue） I. experimental purpose 1. Master the principle and method of preparing acetaniline from aniline acetylation. 2. Master the principle of fractionation and the installation and operation of fractionation devices. 3. Consolidate the operation method of recrystallization. 2. Experimental principle Reactive: The role of aromatic acylation in organic synthesis: (1) acetylation is often used to protect beramine and secondary amine functional groups to reduce the sensitivity of aromatic amine to oxidative reagents. (2) after acylation of amino, reduces the amino electrophilic substitu