白酒混标和内标的做法（Liquor blending and internal marking practice）.docVIP

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白酒混标和内标的做法（Liquor blending and internal marking practice）.doc

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白酒混标和内标的做法（Liquor blending and internal marking practice）

白酒混标和内标的做法（Liquor blending and internal marking practice） Liquor gas chromatography Release date: 2010-09-03 click: 21 source: The flavor of liquor is complex, and there are many aromatic components besides ethanol and water. The liquor quality style is composed of the flavor composition of the wine and its quantity ratio relation. The contents of alcohols, esters, organic acids, carbon-based compounds, phenolic compounds and high boiling point compounds in liquor were determined by gas chromatography. One, DNP column determination of alcohol, ester and other components (a) direct injection of DNP column to determine the main alcohols and ester components in liquor Alcohol and ester of white wine are the main fragrances. The advantages of the sample were: simple operation, high accuracy and quick results. The disadvantage is that the extremely small amount of composition is not easy to detect. 1. Preparation of samples 2 percent of the internal system: The internal standard of 2mL - butyl acetate is in the volumetric flask of 1OOmL (because the internal standard is volatile and can be put in a small amount of alcohol in the bottle), with the alcohol content of 55% - 60%. 1-2% sample preparation: Respectively from acetaldehyde, methanol, propanol, sec-butyl alcohol, acetal, n-butyl alcohol, isoamyl alcohol, (hexyl alcohol), each lmL (furfural), ethyl acetate, ethyl butyrate, pentanoic acid ethyl ester, ethyl lactate, ethyl caproate, isoamyl acetate) 2 ml join 1 ooml volumetric flask, with 55% 60% (V/V) ethanol constant volume, after the blending of the prototype. (a little ethanol is added in the volumetric flask to prevent volatilization) The mixing of target: Use the pipette to draw the sample lOmL and the internal standard 5mL, and use the ethanol of 55%-60% (V/V) to be fixed to 1OOmL, and then (can be divided) to be used. Calculation formula of the contents of each component I and the internal standard in the mixed standard: Mi = ci * di * Vi lO00 Ms = cs * v * *