大孔树脂纯化樟树果实红色素的吸附性能研究.PDF

※工艺技术 食品科学 2009, Vol. 30, No. 20 53 大孔树脂纯化樟树果实红色素的吸附性能研究 1 2 , 2 2 2 2 2 桂克印 ，文赤夫 * ，汪 兰 ，王 晶 ，宋卫华 ，夏 凯 ，杨 通 (1.吉首大学城乡资源与规划学院，湖南张家界 427000 ；2 .吉首大学生物资源与环境科学学院，湖南 吉首 4 16000) 摘 要：为提高樟树果实红色素RPCF(red pigment from camphor tree fruit) 的色价，采用静态吸附和动态解吸附的方 法，以吸附率和解吸率为评价指标，研究了大孔树脂吸附与解吸附RPCF 性能。结果表明：D406 树脂对RPCF 的 吸附效果较好，在吸附液pH3 时吸附能力较强；以pH6、流速为1BV/h 的50% 乙醇为洗脱液的洗脱效果较好。经 D406 大孔树脂吸附与解吸附后的色素色价提高了4 .8 倍。 关键词：大孔树脂；樟树果实；天然色素；纯化 Purification of Red Pigment from Camphor Tree Fruits by Macroporous Resin Adsorption 1 2, 2 2 2 2 2 GUI Ke-y in ，WEN Ch i-fu * ，WANG Lan ，WAN G Jing ，SONG Wei-hua ，XIA Kai ，YAN G Tong (1. College of Resource and Planning Science, Jishou University, Zhangj iaj ie 427000, China ； 2. College of Biological Resource and Environmental Science, Jishou University, Jishou 4 16000, China) Abstract ：Red pigment from camphor tree fruits (RPCF) was purified by macroporous resin adsorption to elevate its color value. D-406 resin was chosen from 7 types of macroporou s resins for the purification due to excellent adsorption capability. Subsequently, the optimal adsorption and desorption conditions of RPCF were investigated by single factor test and an enlarged test was carried out to verify them. Results indicated that an optimal purification of RPCF could be achieved through a procedure based on adsorption of sample solution at pH 3, followed by desorption using 50% ethanol solution at pH 6 with a flow rate of 1 BV/h, which resulted in a 4.8-fold increase of color value. Key words ：macroporou s resin ；camph or tree fruit ；natural pigment ；purification 中图分类号：