动物可食性组织中林可霉素和大观霉素残留检测方法_气相色谱法.pdfVIP

, 200 8, 10 ( S2) : 63- 68 Journa l of A gr icu ltura l Sc ience and T echno logy 气相色谱法 陶燕飞, 于 刚, 陈冬梅, 王玉莲, 袁宗辉 ( , (H ZAU ) , , 4 30070) : , , , , , , 30 g / kg, 40 g / kg 30 ~ 3 000 g / kg 40 ~ 10 000g / kg , 73. 2% ~ 85. 7% , , , , : : S816. 17 : A : 10080 864 ( 2008) S200 630 6 D eterm ination of L incom ycin and Sp ectinom y cin in Edib le T issues of An im al by Gas Ch rom atography TAO Y anfe,i YU G ang, CH EN D ongm e,i WANG Y ulian, YUAN Zonghu i ( H uazhong A gricu ltural U n iv ersity, N ational R eference L aboratory of V eterinary D rug R es idues ( H ZAU ) , MO A K ey L aboratory of F ood S afety E valu at ion, W uhan 430070, Ch ina) A bstrac t: Com bined u se of lincomyc in and sp ectinom yc in is commonly in veterinary treatm ent. N onstandard drug u se can lead to obv iou s s ide effect due to the surv iva l residu es in an mi al tissu es and produ cts. It w ou ld influ ence not on ly the processing and produc ing o f an mi al produ cts, but also the health of cu stom ers. A GC m ethod o f s mi u ltaneou s detecting lincomyc in and sp ectinom yc in w as established and va lidated in all an mi a l ed ib le tissues to a low concentra tion ( lmi it o f quantitation) o f 30 g / kg for lincom yc in or 4 0 g / kg fo r spec tinomy cin, resp ec tive ly. T he recover ies o f lincomy cin in the range of 30 ~ 3 000 g / kg and sp ectinom ycin in the range o f 40 ~ 10 000 g / kg sp iked in all tis su es w ere from 73. 2% to 85. 7% . T his m ethod cou ld m on iter lincom yc in and spec tinomy cin s mi u ltaneou sly w ith short ana lysis