湿法磷酸的浓缩（The concentration of wet phosphoric acid）.doc

湿法磷酸的浓缩（The concentration of wet phosphoric acid） The concentration of wet phosphoric acid Font size: | in | small 2010-07-28 09:43 - reading: 237 - comment: 0 I. the principle and method of concentrated process The quality fraction of the phosphoric acid produced by the second water method is only 20% ~ 24% P2O5, and the quality fraction of the phosphoric acid in the production of heavy calcium is 45% P2O5, so the dilute phosphoric acid must be concentrated. The concentration of phosphoric acid is considered to be a difficult operation, this is because the wet process phosphoric acid contains about 2% - H2SO4 and about 2% of H2SiF6 (F), has a strong corrosive, at the same time, in the process of heating concentrated in the dilute phosphoric acid is in supersaturated or saturation state of impurities, along with the increase of concentration of phosphoric acid precipitation, and deposition on the wall surface, it also exists in the process of enrichment of exhaust gas. The method of concentration of phosphoric acid can be divided into two types, namely direct heating and indirect heating evaporation. 1, direct heating evaporation Directly heated evaporation is one of the most simple way for enrichment, phosphoric acid and hot gas straight contact, in terms of its equipment, direct heating evaporation can overcome the middle heat transfer caused by corrosion and scaling problems. The direct heaters that are widely used in the phosphoric acid concentrate have the foam concentration process and the evaporator and the wet wall evaporator. But the use of such devices has declined over the past two decades, mainly because of high fuel costs and emissions standards that fall short of environmental requirements. 2, indirect heating evaporation Indirect heating evaporation is heating steam through a heat transfer medium (such as shell and tube wall) heat transfer to phosphoric acid, because of the phosphoric acid concentration, with the improvement of P2O5 concentration, slu