Co68.25Fe4.5Nb0.8Si11.45B15非晶合金纤维的制备及GMI效应.pdfVIP

研究·分析·实验 Co68.25Fe4.5Nb0.8Si11.45B15 非晶合金纤维的制备及GMI 效应 1 2 武继文 ，张义权 （1. 南京医科大学 基础医学院，江苏南京 210029； 2. 南京师范大学 物理科学与技术学院，江苏南京 210097 ） 摘 要：通过改进现有的熔融抽拉法制备非晶合金纤维的实验装置，成功制得 Co68.25Fe4.5Nb0.8Si11.45B15 合金 纤维。XRD 和 DSC 分析表明，样品材料具有典型的非晶特性。初步测量了制备态纤维的 GMI 效应，发现 GMI 比维持在271.62% 以上，最高可达 310.55% ，远大于铁基纳米晶丝。其中磁电阻比最高达692.91% ，对较高频率 下 GMI 效应起主要作用。 关键词：非晶纤维；熔融抽拉；GMI 效应 中图分类号：O441.6; TG139.+8 文献标识码：A 文章编号：1001-3830(2012)06-0020-04 Preparation and GMI effect of Co68.25Fe4.5Nb0.8Si11.45B15 amorphous fiber 1 2 WU Ji-wen , ZHANG Yi-quan 1. School of Basic Medical Science, Nanjing Medical University, Nanjing 210029, China; 2. School of Physical Science and Technology, Nanjing Normal University, Nanjing 210097, China Abstract: By improving existing experimental device of melt-extraction, Co68.25Fe4.5Nb0.8Si11.45B15 alloy fiber was prepared successfully. XRD and DSC analysis shows that the fiber has typical characteristic of amorphous wire. GMI effect of the amorphous fibers was measured preliminarily, and as a result, it was found that GMI ratio is maintained at more than 271.62%, with maximun value of 310.55%, far greater than that of Fe-based nanocrystalline wires. The magnetic resistance ratio of up to 692.91% is the dominant contribution to the GMI effect in higher frequency. Key words: amorphous fiber; melt-extraction; GMI effect 的关注。由于巨磁阻抗效应具有灵敏度高、响应快、 1 引言 体积小、稳定性好以及非接触性等优点，在微型传 巨磁阻抗 (Giant Magneto-impedance ，GMI) 感器和磁记录等方面具有十分诱人的