Nd-Fe-B磁体烧结致密化过程与致密化机制 Densification Process and Mechanism in Sintered Nd-Fe-B Magnets.pdfVIP

研究 分析 实验 Nd-Fe-B 磁体烧结致密化过程与致密化机制 1 2 刘湘涟 周寿增 1. 湘潭大学 机械工程学院 湖南湘潭 411105 2. 北京科技大学 新金属材料国家重点实验室 北京 100083 摘 要 定量描述了Nd-Fe-B 磁体的烧结致密化过程 分析了有效稀土含量 合金粉末粒度对烧结致密化 过程的影响 研究了 Nd-Fe-B 磁体烧结过程的致密化机制 Nd-Fe-B 磁体烧结致密化过程可分为三个阶段 即 致密化过程迅速进行阶段 缓慢进行阶段 相对稳定阶段 随着烧结温度的上升 第一阶段表现得更为突出 第二阶段对应的烧结时段大大缩短 有效稀土含量的提高 合金粉末粒度的减小显著促进Nd-Fe-B 磁体烧结致 密化过程 主相颗粒重排以及主相颗粒长大与形状适位性变化是Nd-Fe-B 磁体烧结过程的两类主要致密化机制 而且后者对磁体实现完全致密化起着决定性的作用 关键词 Nd-Fe-B 磁体 烧结 颗粒重排及长大 颗粒形状适位性变化 稀土含量 粉末粒度 致密化 中图分类号 TM273 文献标识码 A 文章编号 1001-3830(2006)05-0024-05 Densification Process and Mechanism in Sintered Nd-Fe-B Magnets 1 2 LIU Xiang-lian , ZHOU Shou-zeng 1. School of Mechanical Engineering, Xiangtan University, Xiangtan 411105, China; 2. State Key Laboratory for Advanced Metals and Materials, University of Science and Technology Beijing, Beijing 100083, China Abstract: The densification process and mechanism in sintered Nd-Fe-B magnets have been investigated in this paper. The densification process includes rapid densification stage, slow densification stage and saturation densification stage. A higher effective total rare earth content or a smaller average alloy powder size accelerates the densification process markedly. The densification process progresses through Nd Fe B grain rearrangement, Nd Fe B grain growth 2 14 2 14 and Nd Fe B grain shape accommodation. Moreover, Nd Fe B grain growth and Nd Fe B grain shape 2 14 2 14