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超临界二氧化碳提取肉桂精油的研究-林产化学与工业
23 1 Vol. 23 No. 1
2003 3 Chemistry and Industry of Forest Products Mar . 2003
黄 彪, 刘 雁, 陈 彦, 廖益强
( 福建农林大学 材料工程学院, 福建 南平353001)
HUANG B
: ,
, ,
: 40 35 MPaCO 30 kg/ h(0. 44 0. 02) g/ mL,
2
5. 8% ~ .0% , 5 , ,
: ;
:TS225. 3; S792. 23 : A :0253-2417( 2003) 01- 0059- 04
ST UDY ON EXT RACT ION OF CINNAMON OIL BY SUPERCRIT ICAL
CARBON DIOXIDE
HUANG Biao, LIU Yan, CHEN Yan, LIAO Y-i qiang
( School of Material E ngineering , Fuj ian Agriculture and Forestry University, Nanp ing 353001, China)
Abstract: Extract ion technique of Chinese cinnamon oil by supercritical carbon dioxide method was studied. Factors
affecting extraction yields, such as temperature, pressure, CO flow rate and bulk density of the raw material, were
2
discussed. By orthogonal experiment, opt imal technological conditions were achieved as follow s: extracting tempera-
ture 40 ; extracting pressure 35 MPa; CO flow rate 30 kg/ h; bulk density of raw material(0.44 0.02) g/ mL. Oil
2
yield obtained by this method is 5 times more than that by steam distillation method.The obtained cinnamon oil is of
brownish red color w ith right pure odor.
Key words: supercritical carbon dioxide; cinnamon oil
,
, , ,
;
,
, , ,
[ 1~ 3]
( Cinnamomum cassia Presl) , , , 10
, ,
: 2002- 08- 07
: ( 19 - ) , , , , ,
0 23
, , ( 0. 5% ~ 1.
2%) , , , ,
, ,
1
1. 1
: , , 17. 8% , 0. 43~ 2 mm,
200 g
CO : , 99%
2
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