Characterisation of surface oxygen groups on （描述表面氧组）.pdf

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Characterisation of surface oxygen groups on （描述表面氧组）.pdf

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Characterisation of surface oxygen groups on （描述表面氧组）

J. Serb. Chem. Soc. 76 (5) 757–768 (2011) UDC 666.762.8+541.183+546.21: JSCS–4157 544.723.3+544.032.4 Original scientific paper Characterisation of surface oxygen groups on different carbon materials by the Boehm method and temperature-programmed desorption 1*# 2# 1# ANA M. KALIJADIS , MARIJA M. VUKČEVIĆ , ZORAN M. JOVANOVIĆ , ZORAN V. LAUŠEVIĆ1# and MILA D. LAUŠEVIĆ2# 1Laboratory of Physics, Vinča Institute of Nuclear Sciences, P. O. Box 522, 11000 Belgrade and 2Faculty of Technology and Metallurgy, University of Belgrade, Karnegijeva 4, 11000 Belgrade, Serbia (Received 24 December 2009, revised 27 October 2010) Abstract : The surface characteristics of different carbon materials: activated carbon, carbon felt, glassy carbon and a porous carbon monolith were inves- tigated. The specific surface area was examined by the BET method with N2 adsorption, the amount and the type of surface oxygen groups by Boehm tit- ration as well as by temperature-programmed desorption (TPD). By comparing