高分子印迹固相萃取法测定熏烤肉制品中16种欧盟优控多环芳烃.PDF

4 3 Vol. 4 No. 3 2013 6 Journal of Food Safety and Quality Jun. , 2013 16 1 2 1, 2* 2 朱 琳 , 杨 润 , 马永建 , 刘华良 (1. , 210009; 2. , 210009) 摘 要: 目的 -(MIPSPE-GC/MS) 16 (PAHs)方法 , (SIM), 结果 0.07~0.24 μg/kg, 1~500 μg/L , 0.99910%, 1 5 μg/kg , 16 PAHs 64.24% ~ 111.61%, 10%结论 , 关键词: ; ; ; - Determination of 16 polycyclic aromatic hydrocarbons with European priority in smoked meat by molecularly imprinted solid-phase extraction 1 2 1,2* 2 ZHU Lin , YANG Run , MA Yong-Jian , LIU Hua-Liang (1. School of Public Health, Southeast University, Nanjing 210009, China; 2. Jiangsu Provincial Center for Disease Control and Prevention, Nanjing 210009, China) ABSTRACT: Objective To establish a method for the determination of 16 polycyclic aromatic hydrocarbons (PAHs) with European priority in smoked meat by molecularly imprinted solid-phase extraction and gas chroma- tography-mass spectrometry (MIPSPE-GC/MS). Methods The homogenized sample was extracted ultrasonically with cyclohexane, cleaned up by molecularly imprinted solid-phase extraction catridge (MIPSPE), analyzed by GC/MS under the positive mode