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NEW CARBON MATERIALS Volume 28, Issue 3, Jun 2013 Online English edition of the Chinese language journal Cite this article as: New Carbon Materials, 2013, 28(3):184–190. RESEARCH PAPER Electromagnetic wave absorbing properties of multi-wall carbon nanotube/Fe O hybrid materials 3 4 Hou Cui-ling, Li Tie-hu, Zhao Ting-kai*, Liu He-guang, Liu Le-hao, Zhang Wen-juan Department of Materials Science and Engineering, Northwestern Polytechnical University, Xi’an 710072, China Abstract: Multi-wall carbon nanotube/Fe O hybrids were prepared by a chemical synthesis-hydrothermal treatment method and their 3 4 electromagnetic wave absorbing properties were investigated in the frequency range of 8.2-12.4 GHz (X band). As-prepared hybrids were characterized by transmission electron microscopy, X-ray diffraction and vibrating sample magnetometer. Results indicated that the surface of multi-wall carbon nanotubes was attached to magnetic Fe O nanoparticles. The Fe O content increased and the magnetism of 3 4 3 4 the hybrids was enhanced by increasing the concentrations of Fe2+ and Fe3+ in solution. The minimum reflection loss ( 18.22 dB, 12.05 GHz) was the lowest and the absorbing bandwidth was the widest when the concentrations of Fe2+ and Fe3+ were 0.02 and 0.04 mol/L, respectively. Key Words: Multi-walled carbon nanotubes; Fe O nanoparticles; Electromagnetic wave absorbing property 3 4 1 Introduction as-prepared samples with different contents of Fe2+ and Fe3+ in