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单分散纳米二氧化硅的制备与表征(Preparation and characterization of monodisperse SiO2 Nanoparticles)
单分散纳米二氧化硅的制备与表征(Preparation and characterization of monodisperse SiO2 Nanoparticles)
No.
Volume 27
1 silicate bulletin Vol. 27, No. 1
2008
February
BULLETIN, OF, THE, CHINESE, CERAMIC, SOCIETY
February, 2008
Preparation and characterization of monodisperse nano silica
Fuyuanxiang
Sun Yanhui
Xingxin, GE
(School of chemistry and environment, South China Normal University
Guangzhou
510006)
abstract
Use
Stober sol
2 gel method
The size of the composite was approximately
Monodisperse nano silica spheres from 80 to 150nm
The temperature and ammonia concentration were also discussed
Degree as well as
Effect of TEOS concentration on Synthesis of silica. utilize
The samples were characterized by XRD, IR, SEM, TEM and other means. Result table
bright
The increase of hydrolysis temperature accelerates the maturation of silica particles in solution and induces agglomeration
The increase of ammonia concentration results in an increase in nucleation rate
Hydrolysis rate plus
drama
The particle size of silica increases
The degree of agglomeration also increases.
Increasing the amount of TEOS also results in a slight increase in the particle size of silica
The degree of agglomeration is deepened.
Key word
Monodisperse
Nanometer
SiO2; sol
2 gel method
CLC number
: TQ127
FU, Yuan2xiang, SUN, Yan2hui, GE, X, ing2xin
Document identifier
: A article number
: 100121625 (2008) 0120154206
SynthesisandCharacterization ofMonodisperseSiO 2Nanoparticles
(SchoolofChemistryandEnvironment, SouthChinaNormalUniversity, Guangzhou510006, China)
Abstract:, A, StOber, Sol2gelmethod, has, been, used, to, prepare, monodisperse, and, uniform, 2size, from,,...
Nm silica nanoparticles in this paper. The silica particles were obtained by hydrolysis of tetraethyl
Orthosilicate (TEOS) inethanolmediumuseammoniumascatalystandadetailedstudywascarriedout
On, the, effect, of, different, temperature, amount, of, ammonium, and, TEOS, on,, particle, sizes, and, the
Dispersion., The, structure, of, the, was, examined,
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