Ni-W-纳米Al2O3复合涂层沉积特性的研究.pdfVIP

第37卷 第1期 人 工 晶 体 学 报 Vo1．37 No．1 2008年2月 JOURNAL OF SYNTHETIC CRYSTALS February．2008 Ni-W-纳米Al2 o3复合涂层沉积特性的研究 朱邦同，吴玉程，李 云，舒 霞，王莉萍，黄新民 (合肥工业大学材料科学与工程学院，合肥23ooo9) 摘要：采用复合电镀的方法制备出Ni—W一纳米AI 0，复合涂层，研究了AI 0，添加量、温度和超声波分散等沉积条 件对复合涂层沉积特性如沉积速率、AI 0，复合量和显微硬度的影响。结果表明，随着纳米AI 0 添加量的增加， 复合涂层的沉积速率、AI 0，复合量和显微硬度不断增加，但当AI 0，添加量达到15g／L时沉积速度开始下降， A1zO，添加量达到17·5g／L时硬度开始下降；适宜的镀液温度大约为80~C，超声波分散时间大约为lh。 关键词：沉积条件；Ni—w一纳米A1 0，复合涂层；沉积特性 中图分类号：TB33 文献标识码：A 文章编号：1000-985X(2008)01-0129-05 Study on Co-deposited Characteristics of Ni．W．nano Al2 O3 Composite Coatings ZHU Bang—tong，WU Yu—cheng ，LI Yun，SHU Xia，WANG H-ping ，HUANG Xin—min (School of Material Science and Engineering，Hefei University of Technology，Hefei 230009，China) (Received9 4P 2007，accepted 30May2007) Abstract：Ni—W—nano A12 03 composite coatings were CO—deposited by composite plating method．The effects of A12 03 concen~ation in electrolyte，temperature and ultrasonic stirring on the CO—deposited characteristics such as deposition rate，A12 O3 content in coating and micro—hardness were investigated． The results show that deposition rate，A12 03 content in coating and micro—hardness increase with the increase of A12 03 concentration in electrolyte，but deposition rate will decrease when A12 O3 concentration in electrolyte reaches 15s／L．Micro—hardness will decrease when A12O3 concentration in electrolyte reaches 17．5g／L．The appropriate temperature at about 80℃ and time of ultrasonic disperse in about lh were determined． Key words：deposited parameters；Ni—W—nano A12 03 composite coating；deposited characteristics 引 言 近年来随着纳米科技 ， 的发