中空催化剂载体生产工艺研究分析.docVIP

SHANDONGＵＮＩＶＥＲＳＩＴＹ　ＯＦ　ＴＥＣＨＮＯＬＯＧＹ 毕业论文 中空催化剂载体生产工艺研究 学 院： 化学工程学院 专 业： 化学工程与工艺 学生姓名： 王晓杰 学 号： 12120802186 指导教师： 王 捷 2016 年 6 月  摘 要 活性氧化铝具备多孔性 本试验做了以下三个方面工作：选择海藻酸钠和氯化钙反应生成明胶做种子；滚动成型，制作具有氧化铝外壳的氧化铝小球；分析氧化铝小球的堆积密度、吸水性、强度。 选择海藻酸钠和氯化钙反应生成的明胶作为种子，采用了的方法，制造了一种氧化铝球。经高温煅烧，球内种子从而制中空型氧化铝球。测试此种氧化铝球的堆积密度、吸水性、强度等指标。 关键词：海藻酸钠 氧化铝 中空 Abstract Activated alumina catalyst carrier can be a good , high specific surface area which has a good adsorption characteristics and have a porous , hollow spherical manufacturing active catalyst carrier having a great industrial value. The tests done the following three aspects of the work: Select gelatin sodium alginate and calcium chloride react for seed ; roll forming to produce alumina having an alumina ball housing ; analysis of bulk density of the alumina pellets , water absorption, strength. Select sodium alginate and calcium chloride produced by the reaction of gelatin as a seed , using a roll molding method , an active alumina manufactured housing alumina pellets . And then by high temperature calcination, evaporate thus produce seeds inside a hollow sphere alumina pellets.Bulk density , water absorption and strength of alumina balls of this index test found that different diameter alumina balls , after calcination , the packing density is significantly reduced , at least to reduce 0.2772g/ml, reduced maximum 0.3007g / ml, respectively can be seen, the greater the diameter of the alumina balls , bulk density , the more the reduced amount ; hollow alumina spheres water absorption of about 0.5 , when the diameter in the range 4.0-4.5mm relatively water absorption high , 3.5-4mm in diameter in the range of relatively low water absorption ; hollow size under the same conditions , the strength of the hollow aluminum ball and the wall thickness increases gradually increased , the greater the thickness , the greater the pressure . But on the whole smaller than t