原创力文档crystallization, transport and magnetic properties of the amorphous (fe1–xmnx)75p15c10 alloys非晶的结晶、运输和磁性(fe1-xmnx)75 p15c10合金.pdfVIP
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crystallization, transport and magnetic properties of the amorphous (fe1–xmnx)75p15c10 alloys非晶的结晶、运输和磁性(fe1-xmnx)75 p15c10合金
Journal of Crystallization Process and Technology, 2012, 2, 105-110 105
/10.4236/jcpt.2012.23013 Published Online July 2012 (http://www.SciRP.org/journal/jcpt)
Crystallization, Transport and Magnetic Properties of the
Amorphous (Fe Mn ) P C Alloys
1–x x 75 15 10
1* 2 3 2
Md. Kamruzzaman , Md. Abu Sayem Karal , Dilip Kumar Saha , Feroz Alam Khan
1Department of Physics, Begum Rokeya University, Rangpur, Bangladesh; 2Bangladesh University of Engineering and Technology
(BUET), Dhaka, Bangladesh; 3Materials Science Division, Atomic Energy Center, Dhaka, Bangladesh.
*
Email: mkzaman_phybuet@, {asayem221, fakhan}@phy.buet.ac.bd
Received April 6th, 2012; revised May 5th, 2012; accepted May 14th, 2012
ABSTRACT
The amorphous (Fe Mn ) P C (0 ≤ x ≤ 0.30) alloys were prepared by the standard melt spinning technique and
1–x x 75 15 10
investigated their crystallization, thermal, transport and magnetic properties. Crystallization was observed from 400˚C
to 650˚C with an interval 50˚C within 30 minutes annealing time by XRD. The as-cast samples were amorphous in na-
ture. Annealing 400˚C to 450˚C samples showed the mixed bcc Fe and amorphous structures. The lattice parameter “a”
was varied from 2.855 to 2.859 Å but above 450˚C, samples contained hexagonal, FeP and FeC structures. The lattice
parameters “a” and “c” were varied from (5.016 - 5.036) Å and (13.575 - 13.820) Å, respectively. Average crystallite
size was found to vary from 8 to 48 nm. Crystallization temperature and weight change were observed by differential
thermal analysis and thermogravimetric analysis, respectively. Crystallizat
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