degradation of diclofenac in molecularly imprinted polymer submicron particles by uv light irradiation and hcl acid treatment退化的双氯芬酸分子印迹聚合物亚微米粒子通过紫外线照射和盐酸酸治疗.pdfVIP

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degradation of diclofenac in molecularly imprinted polymer submicron particles by uv light irradiation and hcl acid treatment退化的双氯芬酸分子印迹聚合物亚微米粒子通过紫外线照射和盐酸酸治疗.pdf

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degradation of diclofenac in molecularly imprinted polymer submicron particles by uv light irradiation and hcl acid treatment退化的双氯芬酸分子印迹聚合物亚微米粒子通过紫外线照射和盐酸酸治疗

Journal of Water Resource and Protection, 2011, 3, 643-654 doi:10.4236/jwarp.2011.39074 Published Online September 2011 (http://www.SciRP.org/journal/jwarp) Degradation of Diclofenac in Molecularly Imprinted Polymer Submicron Particles by UV Light Irradiation and HCl Acid Treatment 1 2* 3 3 Mohammad Hassanzadeh-Khayyat , Edward P. C. Lai , Kerim Kollu , Banu Ormeci 1 Pharmaceutical Sciences Research Center, Department of Pharmaceutical Chemistry, University of Medical Sciences, Mashhad, Iran 2Department of Chemistry, Carleton University, Ottawa, Canada 3Department of Civil and Environmental Engineering , Carleton University, Ottawa, Canada E-mail : edward_lai@carleton.ca Received July 2, 2011; revised August 3, 2011; accepted September 2, 2011 Abstract A new molecularly imprinted polymer (MIP) was synthesized by precipitation polymerization using di- clofenac (DFC) as a template. Binding characteristics of the MIP particles were evaluated by equilibrium binding experiments. DFC-MIP aqueous suspension and non-imprinted polymer (NIP) suspension were ex- posed to monochromatic UV light (253.7 nm) from low-pressure mercury lamps. UV-visible spectropho- tometry (especially absorbance at 276 nm) showed that the DFC inside MIP particles degraded completely. After DFC-MIP suspension exposure to UV light the particles were completely regenerated after washing with water at least six times. The regenerated MIP particles rebounded considerable amou