本科毕业论文(化学吸附).docVIP

安 徽 农 业 大 学 毕 业 论 文(设计) 论文题目 一种简易测定环氧乙烷解吸速率常数的方法及其验证 姓 名 学 号 院 系 理学院 专 业 应用化学 指导教师 职 称 副教授 中国·合肥 二零一三年六月 安徽农业大学学士学位论文(设计)开题报告 课题名称 一种简易测定环氧乙烷解吸速率常数的方法及其验证 课题来源 创新基金 学生姓名 专业 应用化学 学号 指导教师姓名 职称 副教授 研究内容 本实验以环氧乙烷在医用纱布表面吸附为例。先将若干相同纱布在相同环境中进行吸附处理相同时间，再通风解吸不同时长，检测经不同解吸时长后纱布的环氧乙烷残留。根据气-固理想吸附层解吸速率公式，利用实验测得的数据进行拟合，得到解吸速率常数。通过测得的解吸速率常数计算某一解吸时长所应对应的环氧乙烷残留量，并进行实验验证，即比较计算的理论残留量与实际检测残留量之间的偏差，从而评估该方法的可靠性。 研究计划 2012.11月～2012.12月 进行了相关实验背景和文献资料的收集整理，初步确定实验方案。 2013.2月～2013.3月 对实验中涉及到的具体实验仪器与化学药品进行初步汇总。 2013.3月～2013.4月 对实验所需原料、药品、仪器进行采购。 2013.3月～2013.5月 具体实验阶段，通过实验，测定拟合环氧乙烷解吸速率常数所需的各数据。 5） 后期阶段，将相关的研究和实验结果整理形成论文形式。 特色创新 本实验以气固吸附解吸解吸速率方程为基础，通过数学变换，将实验中难以测得的量转化为易于直接观测的量，从而得到数据对方程进行拟合。 指导教师意见 同意开题 教研室意见 院系意见 主要领导签名： 年 月 日 目 录 中文摘要1.1 数据的拟合·····························································································2 1.2 环氧乙烷的检测·······················································································2 1.3 环氧乙烷的制取·······················································································3 2 实验用品···································································································2 2.1 主要仪器·································································································3 2.2 试剂·······································································································3 3 实验内容····································································································3 3.1 试剂配制·································································································3 3.2 吸附及解吸处理·······················································································4 3.3 残留检测································································································ 4 3.4 验证·························