连红愈创灵中肉桂酸含量测定（Determination of cinnamic acid content in Lian Bi Ling Ling）.docVIP

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连红愈创灵中肉桂酸含量测定（Determination of cinnamic acid content in Lian Bi Ling Ling）.doc

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连红愈创灵中肉桂酸含量测定（Determination of cinnamic acid content in Lian Bi Ling Ling）

连红愈创灵中肉桂酸含量测定（Determination of cinnamic acid content in Lian Bi Ling Ling） Even the content of cinnamic acid in determination of guaiacol red spirit Update: 2010-08-12: Zhang Ling Shi Yanzeng Xu Xingang single click Weihua Xu Benming Li Chunling The red spirit in guaiacol cinnamic acid content were determined by dual wavelength TLC scanning method, the method is simple and rapid, and has better accuracy and precision. Keywords safflower guaiac Ling; cinnamon; cinnamic acid; TLC scanning method Even the red spirit guaiac for traditional Chinese medicine topical liniment, from safflower, cinnamon, forsythia, cortex moutan and formula, has the functions of promoting blood circulation and removing blood stasis, detumescence and acesodyne, Qufushengji, swelling and pain, for trauma traumatic injury syndrome, three types of drugs for traditional Chinese medicine. To ensure the quality of preparation, using dual wavelength TLC scanning method for determination of cinnamic acid. 1 instruments and reagents CS-930 scanner (Shimadzu Corporation), PBQ-I thin layer automatic coater (Chongqing Nanan Sony Experimental Electric Appliance Factory), quantitative capillary (Drummond plant); cinnamic acid control (China control of pharmaceutical and Biological Products Institute), cinnamon (purchased from Jinan medicine Station, by the student chamber researcher Peng Guangfang identification of herbs with the Pharmacopeia); reagents used were of analytical grade. Methods and results 2 2.1 samples for sample preparation: the precise amount of red spirit guaiac 10ml, pH adjusted to 2 with hydrochloric acid, ethyl ether saturated water extraction 4 times, 10ml/ times. The combined ether extract, evaporated and the residue dissolved with ethanol and quantitatively transferred to 5ml volumetric flask, and dilute to the mark, shake, as the testsolution. 2.2 cinnamic acid standard solution preparation: precision weighing control 2mg cinnamic acid, methanol dissolved, transferred to a 2ml volu