c6h2（no2）3onh4的晶形控制与性能表征 crystal form control and properties characterization of c6h2(no2)3onh4.pdfVIP

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c6h2（no2）3onh4的晶形控制与性能表征 crystal form control and properties characterization of c6h2(no2)3onh4.pdf

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c6h2（no2）3onh4的晶形控制与性能表征 crystal form control and properties characterization of c6h2(no2)3onh4

2016 08 INITIATORS PYROTECHNICS 2016 4 文章编号：1003-1480201604-0040-04 C H (NO ) ONH 的晶形控制与性能表征 6 2 2 3 4 侯聪花，姜雪梅，贾新磊，王晶禹 030051 摘要：C H (NO ) ONH 6 2 2 3 4 SEMXRDDSC 0.5m X 4.701 kJ·mol-113.63 (H50)7.25% 关键词中图分类号：TQ564 文献标识码：A Crystal Form Control and Properties Characterization of C H (NO ) ONH 6 2 2 3 4 HOU Cong-hua , JIANG Xue-mei , JIA Xin-lei,WANG Jing-yu School of Chemical and Environmental Engineering, North Univercity of China, Taiyuan, 030051) Abstract ：The insensitive explosive compound ammonium picrate (C H (NO ) ONH ) with picric acid and ammonia was 6 2 2 3 4 prepared. On this basis, the effects of crystal-growing controlling agent PVA on the morphology and performance of ammonium picrate was studied. Meanwhile, the performance test and analysis were carried out by SEM, XRD, DSC and impact sensitivity test. The results showed that the performance of ammonium picrate was greatly improved through controlling crystal form. Compared with the sample, the diameter of ammonium picrate (PVA) is about 0.5μm of spherical shape , while the characteristic X-ray diffraction peaks and characteristic peaks were not changed, the activation energy was increased 4.701kJ•mol-1 , the thermal explosion critical temperature was increased 13.63℃and characteristics drop value (H50) was increased