a facile and convenient synthesis of some novel hydrazones, schiff’s base and pyrazoles incorporating thieno[2,3-b]thiophenes一个简单和方便一些新奇的腙的合成希夫碱和摘要将thieno[2,3 b]噻吩.pdfVIP

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a facile and convenient synthesis of some novel hydrazones, schiff’s base and pyrazoles incorporating thieno[2,3-b]thiophenes一个简单和方便一些新奇的腙的合成希夫碱和摘要将thieno[2,3 b]噻吩.pdf

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a facile and convenient synthesis of some novel hydrazones, schiff’s base and pyrazoles incorporating thieno[2,3-b]thiophenes一个简单和方便一些新奇的腙的合成希夫碱和摘要将thieno[2,3 b]噻吩

Int. J. Mol. Sci. 2011, 12, 7824-7834; doi:10.3390/ijm OPEN ACCESS International Journal of Molecular Sciences ISSN 1422-0067 /journal/ijms Article A Facile and Convenient Synthesis of some Novel Hydrazones, Schiff’s Base and Pyrazoles Incorporating Thieno[2,3-b]thiophenes Yahia Nasser Mabkhot *, Assem Barakat *, Abdullah Mohammed Al-Majid, Zeid Abdullah Al-Othman and Abdullah Saleh Alamary Department of Chemistry, Faculty of Science, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi Arabia; E-Mails: amajid@.sa (A.M.A.-M.); zaothman@.sa (Z.A.A.-O.); alamary1401@ (A.S.A.) * Authors to whom correspondence should be addressed; E-Mails: yahia@.sa (Y.N.M.); ambarakat@.sa (A.B.); Tel.: +96614675884; Fax: +96614675992. Received: 8 October 2011; in revised form: 25 October 2011 / Accepted: 31 October 2011 / Published: 11 November 2011 Abstract: A facile and convenient synthesis of some novel hydrazones, schiff’s base and pyrazoles from thieno[2,3-b]thiophene derivatives 1 have been achieved in high yields assisted by microwave and classical methods. The structures of all the title compounds have been elucidated by elemental analysis, IR, MS, 1H-NMR and 13C-NMR. Generally, these findings represent a new class of sulfur and nitrogen moieties that should also be of interest as new materials. Keywords: bicyclic compounds; hydrazone; thieno[2,3-b]thiophenes; heterocycles; schiff’s