conversion of natural aldehydes from eucalyptus citriodora, cymbopogon citratus, and lippia multiflora into oximes gc-ms and ft-ir analysis ？从桉树citriodora转换自然醛,cymbopogon citratus,和lippia野蔷薇成肟gc - ms和傅立叶变换红外光谱分析.pdfVIP

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conversion of natural aldehydes from eucalyptus citriodora, cymbopogon citratus, and lippia multiflora into oximes gc-ms and ft-ir analysis ？从桉树citriodora转换自然醛,cymbopogon citratus,和lippia野蔷薇成肟gc - ms和傅立叶变换红外光谱分析.pdf

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conversion of natural aldehydes from eucalyptus citriodora, cymbopogon citratus, and lippia multiflora into oximes gc-ms and ft-ir analysis ？从桉树citriodora转换自然醛,cymbopogon citratus,和lippia野蔷薇成肟gc - ms和傅立叶变换红外光谱分析

Molecules 2009, 14, 3275-3285; doi:10.3390/molecule OPEN ACCESS molecules ISSN 1420-3049 /journal/molecules Article Conversion of Natural Aldehydes from Eucalyptus citriodora, Cymbopogon citratus, and Lippia multiflora into Oximes: GC-MS † and FT-IR Analysis Igor W. Ouédraogo 1, Michael Boulvin 2, Robert Flammang 2, Pascal Gerbaux 2 and Yvonne L. Bonzi-Coulibaly 1,* 1 Laboratoire de Chimie Organique: Structure et Réactivité; UFR-SEA, Université de Ouagadougou, 03 BP 7021, Ouagadougou 03, Burkina Faso 2 Laboratoire de Chimie Organique, Centre de Spectrométrie de Masse, Université de Mons, Place du Parc 20, B-7000 Mons, Belgique ; E-mail: pascal.gerbaux@umh.ac.be (P.G.) † Dedicated to the memory of Prof. Guy Ourisson, Strasbourg, France (1926-2006), an inspiring mentor. * Author to whom correspondence should be addressed; E-mail: bonziy@univ-ouaga.bf; Tel.: +226 50 30 70 34; Fax: +226 50 30 72 42. Received: 20 July 2009; in revised form: 11 August 2009 / Accepted: 26 August 2009 / Published: 31 August 2009 Abstract: Three carbonyl-containing extracts of essential oils from Eucalyptus citriodora (Myrtaceae), Cymbopogon citratus (Gramineae) and Lippia multiflora (Verbenaceae) were used for the preparation of oximes. The reaction mixtures were analyzed by GC-MS and different compounds were identified on the basis of their retention times and mass spectra. We observed quantitative conversion of aldehydes to their corresponding oximes with a purity of 95 to 99%. E and Z stereoisomers of