原创力文档flow-injection coulometric detection based on ion transfer and its application to the determination of chlorpromazine流动注射电量检测基于离子传输和应用氯丙嗪的决心.pdfVIP
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flow-injection coulometric detection based on ion transfer and its application to the determination of chlorpromazine流动注射电量检测基于离子传输和应用氯丙嗪的决心
Sensors 2008, 8, 3678-3688; DOI: 10.3390/s8063678
OPEN ACCESS
sensors
ISSN 1424-8220
/sensors
Article
Flow-Injection Coulometric Detection Based on Ion Transfer
and Its Application to the Determination of Chlorpromazine
Joaquín A. Ortuño *, Antonio Gil and Concepción Sánchez-Pedreño
Department of Analytical Chemistry, Faculty of Chemistry, Campus de Espinardo, University of
Murcia, 30071-Murcia, Spain
*Author to whom correspondence should be addressed; E-mail address: jortuno@um.es
Received: 2 April 2008; in revised form: 29 May 2008 / Accepted: 29 May 2008 /
Published: 1 June 2008
Abstract: A flow-injection coulometric method for the determination of chlorpromazine
based on ion transfer into a plasticized poly(vinyl chloride) (PVC) membrane, was
developed. The detector used consists of a flow-through cell that incorporates a plasticized
poly(vinyl chloride) (PVC) membrane which contains tetrabutylammonium
tetraphenylborate as electrolyte. The membrane is located between the flowing solution and
an inner aqueous electrolyte solution. Two pairs of electrodes, each pair formed by a
reference electrode and a working electrode, are used, one pair in each solution. The
potential between the reference electrodes was controlled by a four-electrode potentiostat
with ohmic drop compensation. A potential step capable of producing the transfer of the
chlorpromazine ion into the membrane wa
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