synthesis and insecticidal activities of new ester-derivatives of celangulin-v新酯衍生物的合成及杀虫活动celangulin-v.pdfVIP

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synthesis and insecticidal activities of new ester-derivatives of celangulin-v新酯衍生物的合成及杀虫活动celangulin-v.pdf

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synthesis and insecticidal activities of new ester-derivatives of celangulin-v新酯衍生物的合成及杀虫活动celangulin-v

Int. J. Mol. Sci. 2011, 12, 9596-9604; doi:10.3390/ijm OPEN ACCESS International Journal of Molecular Sciences ISSN 1422-0067 /journal/ijms Article Synthesis and Insecticidal Activities of New Ester-Derivatives of Celangulin-V Jiwen Zhang, Zhan Hu, Shenkun Li and Wenjun Wu * Institute of Pesticide Science, Northwest AF University, Yangling, Shaanxi 712100, China; E-Mails: nwzjw@ (J.Z.); huzhan123cn@ (Z.H.); saintkun001@ (S.L.) * Author to whom correspondence should be addressed; E-Mail: wuwenjun@; Tel.: +86-29-8709-2191; Fax: +86-29-8709-3987. Received: 17 August 2011; in revised form: 28 October 2011 / Accepted: 15 December 2011 / Published: 20 December 2011 Abstract: In order to develop new biorational pesticides, ten new 6-substituted ester derivatives of Celangulin-V were designed and synthesized. The structures of the new derivatives were confirmed by IR, 1H-NMR, 13C-NMR and ESI-MS spectral analysis. Insecticidal activities of these compounds were tested against the third-instar larvae of Mythimna separata . Two derivatives (1.1, 1.2) showed higher insecticidal activities than Celangulin-V, with mortality of 75.0% and 83.3%, respectively. While four compounds (1.3, 1.4, 1.7, 1.8) denoted lower insecticidal activities, the others (1.5, 1.6, 1.9, 1.10) revealed no activities at