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显色试剂大全(Reagent kit)
显色试剂大全(Reagent kit)
Reagent kit
Chromogenic reagent
Chromogenic agents can be divided into two broad categories: one is a general color agent for checking general organic compounds; the other is a proprietary color developer based on the classification of compounds or the design of specific functional groups. There are many kinds of color developing agents. This chapter can only list some common chromogenic agents.
L. universal color developer
1. There are four kinds of commonly used sulfuric acid solution: sulfuric acid water (1:1) solution; sulfuric acid methanol or ethanol (1:1) solution; 1.5mol / L 0.5-1.5mol / L sulfuric acid solution with ammonium sulfate solution, spray 110oC after baking 15min, different organic compounds show different colors.
0.5%. The chloroform solution of iodine is yellow brown to many compounds.
The neutral 0.05% Potassium Permanganate solution easy reduction of compounds in the pink background show yellow.
The basic Potassium Permanganate reagent reductive compound in the pale red background show yellow.
Potassium Permanganate I:1% solution solution solution; II: 5% sodium carbonate solution; solutions I and II mixed application.
The Potassium Permanganate 1.6% Potassium Permanganate spray reagent acid concentrated sulfuric acid solution (dissolved attention to prevent explosion), after spraying 180oC heating in thin layer of 15 ~ 20min.
The acidic potassium dichromate injection 5% potassium dichromate sulfuric acid solution, if necessary, 150oC baked thin.
The 5% phosphomolybdic acid ethanol solution after spraying 120oC baking, reductive compound blue, then ammonia smoked, the background becomes colorless.
The potassium ferricyanide and ferric chloride reagent reducing substances blue, then sprayed 2mol / L hydrochloric acid solution, then enhance the blue.
Solution I:1% potassium ferricyanide solution; solution II: 2% ferric chloride solution;
The solution I is mixed with the solution II before use.
2. proprietary color developer
B
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