浙贝母提取工艺的优化选择（Optimization of extraction process of Fritillaria thunbergii Miq）.docVIP

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浙贝母提取工艺的优化选择（Optimization of extraction process of Fritillaria thunbergii Miq）.doc

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浙贝母提取工艺的优化选择（Optimization of extraction process of Fritillaria thunbergii Miq）

浙贝母提取工艺的优化选择（Optimization of extraction process of Fritillaria thunbergii Miq） Optimization of extraction process of Fritillaria thunbergii Miq Update Date: 2009-07-29 Click: su * * * * Cheng Yanyang, Chen Bin Taking the content of total alkaloid as index, orthogonal test was used to investigate the effect of extraction solvent, solvent concentration, treatment methods and extraction times on the extraction of total alkaloids. The results showed that the optimum extraction process of Fritillaria thunbergii was 2 times with 95% ethanol, 1 h each time, and the whole granule was extracted. The amount of solvent was 6 times, and the medicinal material was not treated with alkali. Keywords Fritillaria thunbergii Miq; total alkaloids; extraction process; orthogonal test; The effect of the fritillary bulb is clearing away heat, moistening the lung, resolving phlegm and relieving cough, and the main active ingredient, Fritillaria, has the function of resolving phlegm and relieving cough (1). In order to establish a scientific and reasonable extraction process and to ensure the extraction efficiency of active ingredients, the optimum extraction process was studied by orthogonal test with total alkaloid content as the index. 1 instrument and reagent Hualian CARY-1 UV spectrophotometer, Zhejiang Fritillaria purchased from Guangzhou medicine company, peimine control provided by China control of pharmaceutical and biological products, reagents used were of analytical grade. 2 methods and results 2.1 extraction of samples: 8 pieces of Fritillaria thunbergii Miq., each 30 g, processed and extracted according to the condition of Table 1. The final volume of the extract was determined as the sample solution. 2.2 determination of total alkaloids [2] 2.2.1 standard curve preparation: precise determination of Fritillaria a, standard 5.1 mg, set 50 mL capacity bottle, chlorination, dissolution to scale, shake well, as a control solution. From 5, 1, respectively, the precision of 1.5, 2,