低温合成镁铝尖晶石的研究-福州大学学报.PDFVIP

36 3 () Vol. 36 No. 3 2008 6 Journal of Fuzhou Un iversity( Natural Science) Jun. 2008 : 000- 2243(2008) 03- 0403- 05 , , , (, 350002) : , ( 800~ 500 e ) , XRD SEM . : 800 e , , , , , ; 400e , , , . SEM XRD , 500 e , , . : ; ; : TQ 75 : A Synthesis ofM g-Al spinel at low temperature LIU Sheng, ZHAO Zh i- dong, YU Yan, HUANG Y an ( College ofM aterials Science and Engineering, Fuzhou University, Fuzhou, Fujian 350002, Ch ina) Abstract: Mg-A l sp inelw as synthesized by using w aste alum inum slag and (MgCO ) Mg(OH ) 5H O 3 4 2 2 as main startingmaterials. The form ing course at low temperature ( from 800 to 500 e ) w as character- ized viaXRD and SEM techn iques. The results show that the characteristic peaks ofMg-A l sp inel can be detected at the temperature of 800 e , but the strength is low and be obviously broadened. It suggests that the grains ofMg-A l spinel begin to form and its content is low at this temperature. The diffraction peak strength ofMg-A l spinel increasesw ith increasing temperature which shows that its content is in- creasing. SEM observation results are in according w ithXRD analysis. A t the temperature of 500 e , Mg-A l spinel crystals grow maturely, arrange compactly and take on typ ical octahedral look. Keywords: Mg-A l spinel; low temperatu