实验 2 蒸馏和分馏实验比较（Experiment 2 Comparison of distillation and fractionation experiments）.doc

实验 2 蒸馏和分馏实验比较（Experiment 2 Comparison of distillation and fractionation experiments） Experiment 2 Comparison of distillation and fractionation experiments (acetone water mixture separated) Ask questions before the experiment: How many parts does the 1. fractionation unit consist of? Whats the difference between distillation and distillation? 2. the main purpose of fractionation First, the purpose of the experiment: (1) to understand the basic principles of distillation and fractionation, the scope of application, the conditions under which distillation is used, and what conditions are used for fractionation. (2) proficiency in the installation and use of distillation units. (3) grasp the working principle of fractionating column and simple fractionation operation under atmospheric pressure. The basic principle of distillation and fractionation is the same, is the use of boiling point of organic matter is different, in the distillation process of low boiling components after steaming, high boiling components after steaming, so as to achieve the purpose of separation and purification. The difference is that with the help of fractionation is the distillation column without a series of repeated distillation completed once (fractionation is distilled), the application scope is different, the distillation mixed boiling point liquid component is 30 DEG C, it can be separated, and completely separated from the boiling point to the difference of 110 DEG C. Fractionation allows separation and purification of mixtures of miscible liquids (even a boiling point of only 1-2 DEG C) near boiling point. Two 、 experimental principle Distillation - the joint operation of heating a liquid substance into boiling into steam and condensing it into a liquid. The separation of mixed components by distillation requires that the boiling point difference of the separated components be above 30 DEG C to achieve the purpose of effective separation or purification. Distillation is one of organic