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目 录
中文摘要··································································1
Abstract ··································································3
英文缩略词表 ····························································5
正文 ·······································································6
前言 ·······································································6
1.研究课题的目的 ······················································6
2.课题的理论与实际意义 ·············································6
3. 国内外研究情况简介 ················································8
第一章 抗乳腺增生片的制备工艺研究 ···························10
1.试验材料 ·····························································10
1.1仪器与设备 ·························································10
1.2 材料与试剂 ························································10
2. 制备工艺试验研究 ·················································11
2.1 处方及处方分析 ··················································11
2.2 提取纯化工艺的研究 ············································14
2.3 浓缩干燥工艺的研究 ············································33
2.4 制剂成型工艺的研究 ············································34
2.5 处方及制法 ························································39
2.6 中试放大生产 ·····················································39
3. 讨论 ··································································41
小结 ······································································46
第二章 抗乳腺增生片质量控制研究 ······························47
1.材料与仪器 ··························································47
2. 方法与结果 ··························································47
2.1 鉴别 ································································47
2.2 检查 ································································53
2.3 含量测定 ··························································54
3.讨论 ··································································73
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