白光LED荧光粉外量子效率检测技术研究-中国测试.PDF

第43卷第5期 中国测试 Vol.43 No.5 2017年5月 CHINA MEASUREMENT TEST May袁2017 doi院10.11857/j.issn.1674-5124.2017.05.028 白光LED荧光粉外量子效率检测技术研究 华有杰 渊中国计量大学材料科学与工程学院袁浙江 杭州 310018冤 摘 要院根据荧光粉的发光特性袁对荧光粉外量子效率测试系统中的光路进行改进遥 当测试参比样品和待测样品的反 射光谱时袁通过在光谱仪的狭缝1和传输光纤1之间插入中性衰减片袁对激发光源的发光强度进行有效调节曰当测试 发射光谱时袁则取下该中性衰减片袁使样品的荧光发射强度接近于衰减后的激发光源强度遥 对同一个样品进行10次测 量之后袁发现其测量结果的标准差从3.66降低到0.47袁可有效提高测量精度遥 同时袁研究荧光粉质量浓度对其外量子 效率的影响袁结果表明院荧光粉浓度越低袁外量子效率越高袁其最佳测量浓度约为50%袁此时外量子效率接近于真实值遥 关键词院荧光粉曰白光LED曰中性衰减法曰外量子效率 文献标志码院A 文章编号院1674-5124渊2017冤05-0132-06 Research on the measurement technology of external quantum efficiency of phosphor for white LEDs HUA Youjie 渊College of Materials Science and Engineering袁China Jiliang University袁Hangzhou 310018袁China冤 Abstract: The beam path of external quantum efficiency 渊EQE冤 testing system was improved according to luminescent properties of phosphors. When the reflectance spectra of reference and tested samples were being tested袁 a neutral optical filter was inserted into beam path between slit 1 and transmission fiber 1 in spectrometer. As a result袁 the reflective intensity of excitation light was regulated effectively. When the photoluminescence渊PL冤 spectra were being tested袁 the previous neutral optical filter was taken out. So the PL intensity of tested samples were close to that of reduced excitation light. The standard deviation of EQE values was realized by testing one sample for many times. The value of standard deviation was reduced from 3.66 to 0.47. It indicated that the accuracy of measurement was greatly enhanced. Mor