电感耦合等离子体质谱法测定黑果枸杞中的微量元素-食品安全质量.PDF

6 11 Vol. 6 No. 11 2015 11 Journal of Food Safety and Quality Nov. , 2015 1 2 1, 2* 何 艳 , 燕 娜 , 赵生国 (1. , 730070; 2. , 730010) 摘 要: 目的 (inductively coupled plasma-mass spectrometry, ICP-MS) 方法 , In Bi 结果 0.0060.002 0.0030.0002 mg/kg, 105.5%~118.5% , 0.2%~5.5% , 3~5 结论 关键词: ; ; ; Determination of trace elements in Lycium ruthenicum Murr by inductively coupled plasma mass spectrometry 1 2 1, 2* HE Yan , YAN Na , ZHAO Sheng-Guo (1. College of Geography and Environment Science, Northwest Normal University. Lanzhou 730070, China; 2. Inspection and Quarantine Technology Center, Gansu Entry-Exit Inspection and Quarantine Bureau, Lanzhou 730010, China) ABSTRACT: Objective To establish a method for the determination of four elements (Ga, Ge, Sb, Tl)in Ly- cium ruthenicum Murr by inductively coupled plasma mass spectrometry (ICP-MS). Methods The elements of Ga, Ge, Sb, Tl of Lycium ruthenicum Murr were directly determined by ICP-MS after microwave digestion. Standard mixed solution were added for the standard addition experiment and the recovery rates of Ga, Ge, Sb