硬化水泥净浆纳米划擦行为的荷载效应评价-ingentaconnect.pdfVIP

第39 卷第10 期 王培铭等：背散射电子图像分析在水泥基材料微观结构研究中的应用 · 1701 · 第39 卷第10 期 硅 酸 盐 学 报 Vol. 39 ，No. 10 2 0 1 1 年 1 0 月 JOURNAL OF THE CHINESE CERAMIC SOCIETY October ，2011 硬化水泥净浆纳米划擦行为的荷载效应评价 徐 晶，姚 武 ( 同济大学，先进土木工程材料教育部重点实验室，上海 201804) 摘 要：采用纳米划痕技术研究了硬化纯水泥熟料净浆在划擦过程的弹、塑性变形和摩擦特性，并着重讨论了不同荷载的影响。结果表明：综合压头 压入深度、摩擦因数及弹性恢复率能够有效地对未水化熟料颗粒相和水化产物相进行区别和分析；当荷载低于5 mN 时，材料主要发生弹性变形，以 界面摩擦为主；荷载提高至8 mN 后，水化产物相逐步以塑性变形为主，并产生犁沟摩擦；荷载的提高有利于改善测试数据的离散程度，但高载荷下 在水化产物相某些部位可能发生穿相。 关键词：水泥净浆；纳米划痕；力学性能 中图分类号：TU502 文献标志码：A 文章编号：0454–5648(2011)10–1701–05 网络出版时间：2011–09–27 13:49:21 DOI ：CNKI:11-2310/TQ1349.029 网络出版地址：/kcms/detail/11.2310.TQ1349.029.html Load Effect on Nano-Scratch Behavior of Hardened Cement Paste XU Jing ，YAO Wu (Key Laboratory of Advanced Civil Engineering Materials of Ministry of Education, Tongji University, Shanghai 201804, China) Abstract: The elastic-plastic deformation and tribological properties of hardened paste of pure cement clinker with respect to the load effect were investigated by means of nano-scratch technique. The results indicate that the combined assessment of the indenter pene- tration depth, the coefficient friction and the elastic recovery ratio is efficient for the identification and evaluation of unhydrated clinker particles and hydration products. When the load was below 5 mN, the elastic deformation occurred in the material and the interfacial friction could be dominant. When the load increased to 8 mN, the plastic deformation became dominant in the phase of hydration products as the plough friction took place. In addition, the enhanced load could favor the improvement of the discr