化工设计答辩终稿.ppt

二硫化碳-四氯化碳蒸馏分离过程与精馏塔的设计 团队成员：郭骏、王瑛璞、韩鹏 指导老师：赵海红 设计任务书 1)生产能力：10吨每小时（料液） 2)原料组成：34%的二硫化碳和66%的四氯化碳（摩尔分率，下同） 3) 产品组成：馏出液 97%的二硫化碳，釜液5%的二硫化碳 4) 操作压力：塔顶压强为常压 5) 进料温度：58℃ 6) 进料状况：自定 7) 加热方式：间接蒸汽加热 8) 塔板效率: 0.5； 9) 建厂地址：湖南长沙地区； 10) 其他参数（除给出外）可自选。 目 录 摘要······················································3 前言······················································4 第一章设计方案简介·································6 1.1流程的设计及说明·······························6 1.2已知参数···········································7 1.3 选塔依据··········································7 第二章 设计计算······································9 2.1精馏流程的确定··································9 2.2塔的物料衡算···································· 10 2.3塔板数计算········································11 第三章板式塔主要工艺尺寸设计计算············16 3.1塔工艺条件及物性数据计算···················16 3.2精馏塔气液负荷计算····························20 3.3塔和塔板主要工艺尺寸计算···················20 3.4筛板的流体力学验算····························25 3.5塔板负荷性能图··································29 3.6精馏塔的计算结果总表·························36 第四章精馏塔的附属设备以及接管尺寸·········39 4.1接管设计···········································39 4.2塔总高度计算 ·····································40 4.3热量衡算············································41 4.4再沸器的选择······································44 4.5泵的选型············································44 4.6主要符号说明······································46 参考文献·················································49 设计结果评述与小结··································50 致谢·······················································51 附录·······················································53 人员分配 原料液经过预热器预热后进入精馏塔内。操作时连续的从再沸器中取出部分液体作为塔底产品（釜残液）。再沸器中原料液部分汽化，产生上升蒸汽，依次通过各层塔板。塔顶蒸汽进入冷凝器中全部冷凝，然后进入回流罐，并将冷凝液送回塔顶作为回流液体，其余部分经过冷凝器后被送出作为塔顶产品。为了使精馏塔连续的稳定的进行，流程中还要考虑设置原料槽、产品槽和相应的泵。为了便于了解操作中的情况及时发现问题和采取相应的措施，常在流程中的适当位置设置必要的仪表，比如流量计、温度计和压力表等，以测量物流的各项参数。 设计方案的选定 物料衡算 能量衡算 W=78.44 MW=150.1 aW=0.0251 塔釜 F=53.71 MF=127.48 aF=0.203 进料 D=24.73 MD=78.34 aD=0.941 塔顶 物料衡算kmol/h 平均分子量（g/mol） CS2的质量分率 塔的位