HPLC法测定恩杂鲁胺原料药的含量.PDFVIP

绗紦锛欏嵎绗紪鏈 婀栧寳澶у瀛︽姤锛堣嚜鐒剁瀛︾増锛 锛讹綇锝岋紟锛擄紮銆€ 锛綇锛庯紪銆€ 锛掞紣锛戯紬骞达紤锛戞湀 锛綇锝曪綊锝庯絹锝 锝忥絾 锛綍锝傦絽锝 锛碉綆锝夛綎锝咃綊锝擄綁锝旓綑锛堬籍锝侊綌锝曪綊锝侊綄 锛筹絻锝夛絽锝庯絻锝咃級 锛綇锝栵絽锝嶏絺锝咃綊 锛岋紥锛愶紤锛椼€€ 鏂囩珷缂栧彿锛氾紤锛愶紣锛 锛掞紦锛楋紩锛堬紥锛愶紤锛楋級锛愶紪 锛愶紪锛楋紦 锛愶紨 锛及锛迹娉曟祴瀹氭仼鏉傞瞾鑳哄師鏂欒嵂鐨勫惈閲 鍐附锛屽啹鑿婄孩锛岃儭瀛﹂浄 锛堟姹夊伐绋嬪ぇ瀛﹀寲宸ヤ笌鍒惰嵂瀛﹂櫌锛屾箹鍖 姝︽眽锛旓紦锛愶紣锛楋紨锛 鎽樿锛氫负寤虹珛锛及锛迹娉曟祴瀹氭仼鏉傞瞾鑳哄師鏂欒嵂鐨勫惈閲忥紝閲囩敤锛碉綄锝旓綁锝嶏絹锝旓絽 锛及鈦冿迹锛戯紭锛堬紥锛曪紣 脳锛旓紟锛 锝嶏綅锛岋紩 渭锝嶏級鑹茶氨鏌憋紝浠ョ敳閱囷紞锛愶紟 锛戯紖纾烽吀浜屾阿閽炬憾娑诧紙锛楋紣 鈭讹紦锛愶級涓烘祦鍔ㄧ浉锛屾祦閫熶负 锛戯紟锛 锝嶏棘锛 锝嶏綁锝庯紝杩涙牱閲忎负 锛戯紣 渭锛紟缁撴灉琛ㄦ槑锛屾仼鏉傞瞾鑳虹殑娴撳害鍦 锛戯紥 锛曪紥 渭锝囷紡 锝嶏棘鑼冨洿鍐呬笌宄伴潰绉憟鐜拌壇濂界殑绾挎€у叧绯伙紙锝掞紳锛愶紟锛欙紮锛 锛掞級锛屽钩鍧囧洖鏀剁巼涓猴紮锛欙紟锛戯紭锛 锛戯紣锛愶紟锛戯紣锛咃紙锝 锛濓紦锛夛紝锛诧汲锛 涓猴紣锛庯紨锛 锛愶紟锛曪紖锛庢湰娉曞叿鏈夊垎鏋愰€熷害蹇€佺畝鍗曘€佸噯纭互鍙婁笓灞炴€у己濂界瓑鐗圭偣锛岄€傚悎鎭╂潅椴佽兒鍚噺鐨勬祴瀹氾紟 鍏抽敭璇嶏細鎭╂潅椴佽兒锛涢珮鏁堟恫鐩歌壊璋辨硶锛涘鏍囨硶 涓浘鍒嗙被鍙凤細锛诧紮锛戯紬銆€ 銆€ 鏂囩尞鏍囧織鐮侊細锛°€€ 銆€ 锛わ集锛╋細锛戯紣锛庯紦锛欙紪锛欙紡 锝婏紟锝夛綋锝擄綆锛庯紤锛愶紣锛愨亙锛掞紦锛楋紩锛庯紥锛愶紤锛楋紟锛愶紪锛庯紣锛掞紣 锛わ絽锝旓絽锝掞綅锝夛綆锝侊綌锝夛綇锝 锝忥絾 锝咃綆锝氾絹锝岋綍锝旓絹锝嶏綁锝勶絽 锝冿綊锝曪絼锝 锝勶綊锝曪絿 锝傦綑 锛及锛迹 锛︼讥锛姬 锛綁锛岋鸡锛ワ籍锛э吉锝曪綀锝忥綆锝囷紝锛嫉 锛革綍锝咃綄锝咃綁 锛堬汲锝冿綀锝忥綇锝 锝忥絾 锛ｏ綀锝咃綅锝夛絻锝侊綄 锛ワ綆锝囷綁锝庯絽锝咃綊锝夛綆锝 锝侊綆锝 锛帮綀锝侊綊锝嶏絹锝冿綑锛岋挤锝曪綀锝侊綆 锛╋綆锝擄綌锝夛綌锝曪綌锝 锝忥絾 锛达絽锝冿綀锝庯綇锝岋綇锝囷綑锛岋挤锝曪綀锝侊綆锛旓紦锛愶紣锛楋紨锛岋迹锝堬綁锝庯絹锛 锛★絺锝擄綌锝掞絹锝冿綌锛氾即锝 锝咃綋锝旓絹锝傦綄锝夛綋锝 锝侊綆 锛及锛迹 锝嶏絽锝旓綀锝忥絼锝嗭綇锝 锝旓綀锝 锝勶絽锝旓絽锝掞綅锝夛綆锝侊綌锝夛綇锝 锝忥絾 锝旓綀锝 锝冿綇锝庯綌锝咃綆锝 锝忥絾 锝咃綆锝氾絹锝岋綍锝旓絹锝嶏綁锝勶絽 锝冿綊锝曪絼锝 锝勶綊锝曪絿锛 锛碉綄锝旓綁锝嶏絹锝旓絽 锛及鈦冿迹锛戯紭 锝冿綇锝岋綍锝嶏綆锛堬紥锛曪紣脳锛旓紟锛 锝嶏綅锛岋紩 渭锝嶏級锝楋絹锝 锝曪綋锝咃絼锛庯即锝堬絽 锝嶏綇锝傦綁锝岋絽 锝愶綀锝侊綋锝 锝楋絹锝 锝嶏絽锝旓綀锝忥綆锝侊綄锛嶏紣锛庯紤锛 锝愶綇锝旓絹锝擄綋锝夛綍锝 鈦冿紤 锝勶綁锝堬綑锝勶綊锝忥絿锝咃綆 锝愶綀锝忥綋锝愶綀锝侊綌锝 锝擄綇锝岋綍锝旓綁锝忥綆锛堬紬锛 鈭讹紦锛愶級锛庯即锝堬絽 锝嗭綄锝忥綏 锝掞絹锝旓絽 锝楋絹锝 锛戯紟锛 锝嶏棘 路锝嶏綁锝 锛庯即锝堬絽 锝夛綆锝婏絽锝冿綌锝夛綇锝 锝栵綇锝岋綍锝嶏絽 锝楋絹锝 锛戯紣 渭锛紟 锛达綀锝 锝掞絽锝擄綍锝岋綌锝擄綋锝堬綇锝楋絽锝勶綌锝堬絹锝旓綌锝堬絽锝掞絽锝楋絹锝擄絿锝忥綇锝勶綄锝夛綆锝咃絹锝掞綁锝旓綑 锝忥絾 锝咃綆锝氾絹锝岋綍锝旓絹锝嶏綁锝勶絽锝夛綆锝旓綀锝咃綊锝侊綆锝囷絽锝忥絾 锛戯紥鈥旓紩锛 渭锝囷紡 锝嶏棘锛堬綊锛濓紣锛庯紮锛欙紮锛掞級锛 锛达綀锝 锝侊綎锝咃綊锝侊絿锝 锝掞絽锝冿綇锝栵絽锝掞綑 锝楋絹锝擄紮锛欙紟锛戯紭锛呪€旓紤锛愶紣锛庯紤锛愶紖锛堬綆锛濓紦锛夛紝锝侊綆锝勶疾锛筹激 锝楋絹锝擄紣锛庯紨锛呪€旓紣锛庯紩锛咃紟锛达綀锝 锝嶏絽锝旓綀锝忥絼 锝楋絹锝