电子显微分析（章晓中）教学课件chapter7.pdfVIP

Chapter 4 Complex diffraction patterns twin structure High Order Laue Zones Kikuchi Lines (菊池线） simple electron diffraction pattern All diffraction spots in a simple electron diffraction pattern satisfy Weiss zone law hu+kv+lw=0. The diffraction spots are contributed by the reciprocal points of reciprocal plane (uvw) * which pass through the origin point 0 of the reciprocal lattice space. All spots are in one set of spot grid (2D spot grid). complex electron diffraction patterns • Twin structure (孪晶结构） • High Order Laue Zone （高阶劳厄带） • Kikuchi lines （菊池线) • Superstructure (超结构） • long-period superlattice （长周期结构） • modulated structure （调制结构） • double diffraction （二次衍射） • textured structure （织构） 4.1 The diffraction pattern for twinned crystals （孪晶体） A twinned crystal is one which consists of two or more parts that are oriented in a specific crystallographic relationship to each other. The relationship is normally one in which there is a reflection across a plane (the twin plane) or a rotation of o 180 about the twin axis between the lattices of the two individuals. The special case of the twin axis perpendicular to the electron beam In the figure, hkl represents any general reciprocal lattice point [HKL] and [HKL] the reciprocal lattice t t t h k l hkl vector normal （垂直）to the twin plane (HKL). As a result of twinning on (HKL), hkl (indices for matrix 基体) is rotated by o t t t 180 about [HKL] to h k l (indices for twin). We need t