原创力文档同位素稀释高压液相色谱-串联质谱法测定鱼虾中丙酸睾酮残留量 Determination of testosterone propionate residues in fish and shrimp by high pressure liquid chromatography-tandem mass spectrometry with isotope dilution.pdfVIP
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同位素稀释高压液相色谱-串联质谱法测定鱼虾中丙酸睾酮残留量 Determination of testosterone propionate residues in fish and shrimp by high pressure liquid chromatography-tandem mass spectrometry with isotope dilution
5 1 Vol. 5 No. 1
2014 1 Journal of Food Safety and Quality Jan. , 2014
-
1, 2 1* 1 2 3 2 2
田良良 , 林 洪 , 曹立民 , 蔡友琼 , 王建华 , 黄冬梅 , 史永富
(1. , 266003; 2. ,
( ), 200090; 3. , 266002)
摘 要: 目的 -(high pressure liquid chromatography-tandem mass spectrometry,
HPLC-MS/MS)方法 -D3 ,
, −80 ℃30 min 12000 r/min Eclipse Plus C18 ,
−0.1% , 0.3 mL/min,
结果 0.5~100 ng/mL , 0.9989; 0.5 μg/kg
0.5~10.0 μg/kg , 71.2%~104.5%, 2.26%~5.65% 结论
,
关键词: ; ; ; -
Determination of testosterone propionate residues in fish and shrimp
by high pressure liquid chromatography-tandem mass spectrometry
with isotope dilution
1, 2 1* 1 2 3
TIAN Liang-Liang , LIN Hong , CAO Li-Min , CAI You-Qiong , WANG Jian-Hua ,
HUANG Dong-Mei2, SHI Yong-Fu2
(1. College of Food Science and Engineering of Ocean University of China, Qingdao 266003, China;
2. Fishery Products Quality Inspection and Test Centre (Shanghai), Ministry of Agriculture of China,
East China Sea Fisheries Research Institute, Chinese Academy of Fishery Sciences, Shanghai 200090, China
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