树脂吸附法分离高纯茶多酚新工艺研究-林产化学与工业.PDFVIP

24 4 Vol. 24 No. 4 2004 12 Chemistry and Industry of Forest Products ec. 2004 陈龙胜, 钟世安, 周春山, 雷启福, 高 艺 ( 中南大学 化学化工学院, 湖南 长沙 410083) CHEN L S : ,, pH 1. 5, , AB- 8 , pH 2~ 4 5%, 60%, ,90. 22% : ; ; :TQ281 : A : 0253- 2417( 2004)04- 0065- 03 STU Y ON NEW TECHNOLOGY FOR ISOLAT ING HIGH-PURITY TEA POLYPHENOLS BY MACROPORE RESIN CHEN Long-sheng, ZHONG Sh-i an, ZHOU Chun-shan, LEI Q-i fu, GAO Yi ( College of Chemist ry and Chem ical Eng ineer ing , Ce nt ral Sout h Univ ers ity , Changsha 410083, Chi na) Abstract: A green technology for isolating andpurifying tea polyphenols(TP) from tea leavesby macroporous resinswas studied as follows:soak low-grade tea leaves and filter the crude extract by coarse sand immediately,remove pigment, macromolecular substances and caffeine from crude extract by adjusting pH value,filter again by fine sand and load it onto a column containing macropore resin AB-8 for absorbing TP;TP was desorbed with 5% EtOH eluant of pH value 1.5and 60% EtOH subsequent- ly;dry the solution by spray dryer to obtain high purity TP of purity 90.22%. Key words: tea polyphenols; sand filter; adsorption resin (TP) ,, ,, [1] [2] [ 3] [ 4] TP 3 : , ,, ; , , , :2004- 02- 26 : ( 00NK1010) :( 1980- ) , , , , 66 24 1 1. 1 :( ) ; AB- 8S- 8X- 5 () ; ( ) ; , 100 ;, 100 1.2 100 g , 2 000 mL,pH 3~ 4,1h,, ,pH 1.5, 5 4 h,,, AB- 810 mL ( 800 mm 10 mm) , , pH 2~ 4 5%,60%, ,,AB- 8 90% 1.3