速螨酮在柑橘及土壤中的残留及消解动态-浙江农业学报.PDFVIP

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速螨酮在柑橘及土壤中的残留及消解动态-浙江农业学报.PDF

速螨酮在柑橘及土壤中的残留及消解动态-浙江农业学报

浙江农业学报 (): , Acta Agriculturae Zhej iangensis 18 2 90 ~ 93 2006 速螨酮在柑橘及土壤中的残留及消解动态 徐 浩,赵 华,李 振 (浙江省农业科学院农产品质量标准研究所,浙江 杭州 310021) 摘 要:采用甲醇提取、氧化铝层析柱净化、 测定的分析方法,研究了速螨酮在柑橘和土壤中的残留 GC-ECD 和动态。方法的回收率为80 .98% ~ 100 .78% ,变异系数为1.53% ~ 4 . 51% 。速螨酮在药后 14 d 柑橘全果的 最终残留量 0 .004 mg/ kg。速螨酮在橘皮中半衰期为7 . 17 ~ 10 . 31 d,土壤中为5 . 16 ~ 11.55 d。 关键词:速螨酮;残留;降解;柑橘;土壤 中图分类号: + 文献标识码: 文章编号: ( ) S481 . 8 A 1004 - 1524 2006 02 - 0090 - 04 Study on residue and dissipation dynamics of pyridaben in citrus and soil , , XU Hao ZHAO Hua LI Zhen ( , , , ) Institute of Quality and Standard f or Agro-p roducts Zhej iang Academy of Agricultural Sciences Hangzhou 310021 China : Abstract The degradation and final residue of pyridaben in citrus and soil were studied by the method of methanol extrac- , , tion Al O column purification and GC-ECD detection . The recovery rate of this method ranged from 80 .98% to 100 .78% 2 3 with variation coefficient of 1.53% - 4 .51% . The final residue of pyridaben in full fruit 14 d after the last spraying was below 0 .004 mg/ kg . The half-lives of pyridaben in citrus peel and soil were 7 . 17 - 10 . 31 d and 5 . 16 - 11. 55 d, respec- tively . : ; ; ; ; Key words pyridaben residue degradation citrus soil 速螨酮( )是一种杂环类杀螨剂,化 田间试验 pyridaben 1. 1 学名称为 特丁基 ( 特丁苄基)硫代

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