FeSCO2O3混合催化剂制备煤基碳纳米管研究.pdf

FeS—Co：03混合催化剂制备煤繁碳纳米管 363 FeS—C02 03混合催化剂制备煤基碳纳米管 ofCoal—basedCarbonNanotubewith as Preparation FeS—C0203 Catalyst 范玮卫，吕永康，鲍卫伫，赵娟，范宝芸 太原理工大学煤辩学与技零教育部山魏省重点实验塞，太原030024) FAN Wei-wei，LU Wei—ren，ZHAOJuan，FAN Yong-kang，BA0 Bao-yun ofCoalScienceand ofEducation Laboratory (Key Technology，Ministry andShanxi of 030024，China) Province，TaiyuanUniversityTechnology，Taiyuan 摘要：以煤沟碳源，FeS-CozO；混合扬势催化剂，采用电鞭放电法制备碳纳来管。考察了催讫剂等对碳纳岽管生成的影 1：0．3：0．3下，制备的碳纳米管达到理想效果。且该俄化剂对阳城煤与大同煤的俄化效果近似。同时对FeS，c0203 秀秘镬毙荆凌碳续寒管生长过程孛的接惩遴锷了耪步掇淫。 差键词：煤；FeS-C0203；龟激放电法；碳纳米管 中图分类号：TB383；TQ536 文献标识码：A 文章编号：1001-4381(2008)10—0363—03 nanotubeswere fromcoal arc methodwith as Abstract：Carbon synthesizedby discharge FeS-C0203 effectof onthe ofcarbonnanotubeswas catalyst．Thecatalyst generation CNTswerecharacterized results SEM，HRTEM，Raman showed by spectroscopytechniques．The thatcarbonnanotubescan a whentheratioof WflS1：0．3：0．3． gethighquality coal：FeS：Coz03 Andthe and effectsof onthe coal Coalweresimilar．Inaddition，the catalyst YangchengDatong effectsofFeSand inthe ofcarbonnanotubeswerealso C0203 growth proposed．