先进静高压同步辐射成像技术.pdfVIP

先进静高压同步辐射成像技术 杨文革 华盛顿卡耐基研究院, 地球物理实验室 阿贡国家实验室, 高级先进光源 SSRF, October 2013 Static high pressure tools Diamond Anvil Cells Large Volume Press Diamond anvil cells 1000 mm 70 mm 15 mm 300 mm 13BM-D 35 mm 20 mm 50 mm How to change pressure with DAC ? Gear box Membrane gas control By hand 3d nanoscale tomography for EoS and in situ structure evolution studies Transmission x-ray microscopy (TXM) setup at APS-32IDC and SSRL-6.2 CCD Nano-focusing Sample condenser zone plate stage Beamline capabilities: Full field imaging with 180 degrees data collection; 3d reconstruction with FOV 30 microns and 30 nm resolution 3d Nanoscale phase boundary and valence state mapping XANES-tomo TEM 30 nm feature Beamline capabilities: Full field imaging with 180 degrees data collection; 3d reconstruction with FOV 30 microns and 30 nm require uniform illumination for FOV (diffuser sometimes is used to create incoherent uniform beam) Shape and volume as a function of pressure of a single Sn particle 10 um J. Wang et al. JAP (2012) Nano-imaging Investigation of the formation of planet core with 3d nano-