石墨电化学氧化制备纳米粒子及其表征.PDFVIP

23 4 ( ) Vol. 23No. 4 2002 10 Journal of Huaqiao U niversity ( Natural Science) Oct. 2002 1000- 013(2002) 04-0361-0 翁文桂　陈国华　吴大军　颜文礼 ( , 362011) , . ( PCS) (T EM) ( SAD) X ( XRD) ( FTIR) X (XPS) , 0 nm , . , . , , , 646 16 34 O T Q TB A , . , . , 14 . , , 7 8, 9 . , . 10 , , , . , , , . . 1 1. 1 ( , SES , ) , ( H2 SO4 ) , ( HCl) , ( NaOH) , ( NaCl) , ( Na2CO3) , ( NH4Cl) , . 1. 2 26 ( ) . -100 ( ) , YJ G JEM CX 100 . 7 0 , 1 - 1. kV Nicolet Magna cm 2002-07-27( 1977-) , , ( ) 2002 362 ( Brookhaven Co . Ltd. ) , BI900AT , BI200SM . ( Rigaku) Rotaflex D/ M ax- CXRD . X ( XPS) , VG ESCALAB-, Mg , 400 W, 0 eV. 1. 3 - 1 , 2. 0 , 26 mol L YJ G , ( 1020 V) . , . , . , , , . 1. 0 - 1 , . mol L 2 2. 1 , . , , . , . , , . , , ( , ) 30 . , 7 . . 2. 2TEM , Innova , 14. nm . 160 nm, , 1 . , D . , , 0 nm , 2 . , . , , 1 2TEM , . ( SAD) , , . 4 : 363