7ninb2o69tio2陶瓷的低温烧结和微波介电性能分析 word格式.docxVIP

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7ninb2o69tio2陶瓷的低温烧结和微波介电性能分析 word格式.docx

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7ninb2o69tio2陶瓷的低温烧结和微波介电性能分析 word格式

AbstractWiththegrowingneedsofelectronicproductswithsmallsize,lightweight,more functions，and high integration, using LTCC (Low Temperature co-firing ceramic)technologyto designand fabricatemicrowave componentshasbecomearesearch hotspot. In ordertomeettherequirementofreducingthesizeofthemicrowavecomponents(suchas dielectricresonator,frequencyfilter,oscillator,andsoon),choosingmicrowavedielectric materialswithhigherdielectricpermittivityasthekeymaterialsisessential.Thus,thestudy onlowtemperaturesinteringandmicrowavedielectricpropertiesofceramicswithhigh dielectricpermittivitymeansalottotheproductionofsmall-sizedandhigh-quality microwave components.Thepure7NiNb2O6-9TiO2ceramicsexhibithighdielectricpermittivityof68.7,aQ×f of19300GHz,andacceptableτfof56.6ppm/°C.Buttheyshowahighsinteringtemperature, whichmeanscannotbesinteredwithAg(Cu)electrodes.Soitisessentialtolowerits sinteringtemperature.Inthispaper,theeffectsofadditivesonsinteringtemperatureand microwavedielectricpropertiesof7NiNb2O6-9TiO2ceramicshavebeeninvestigated.The phasesandmicrostructurehavebeenevaluatedusingX-raydiffraction(XRD)andscanning electronmicroscopy(SEM),andthemicrowavedielectricpropertieshavebeenmeasuredby Advantestnetwork analyzer.First,themixtureofCuOandH3BO3wasusedasthesinteringaidstolowerthe sinteringtemperatureof7NiNb2O6-9TiO2ceramics,whichpreparedbysolid-statereaction method.Theresultsshowthatthemixturereducedthesinteringtemperatureof 7NiNb2O6-9TiO2ceramics,buttheeffectisnotenough(1000°C).Moreover,itisobserved thatthedensityofthespecimendecreasedwiththeincreaseofH3BO3content,butincreased with theincrease of CuO content.Then,theCuOwasusedasthesinteringaidstolowerthesinteringtemperatureof 7NiNb2O6-9TiO2ceramics.TheresultsshowthattheCuO-liquidphaseexistsinthe boundaryofgrains,andtheadditionofCuOdoesnotcauseasecondaryphase.TheCuOcan obviouslypromotethedensificationof7NiNb2O6-9TiO2 ceramicswithoutdecreasingthedielectricproperties,andreduceditssinteringtemperaturefrom1,200°Cto935°C.The 7NiNb2O6-9TiO2