agcts印迹凝胶球的制备及性能研究 word格式.docxVIP

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agcts印迹凝胶球的制备及性能研究 word格式.docx

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agcts印迹凝胶球的制备及性能研究 word格式

PreparationandPerfomanceStudyofSilverIonImprintedChitosanGelBeadsSpeciality: Chemical Engineering Master:TongHanTutor: Prof. DongliangLiABSTRACTTheseparationandselectiveenrichmentofsilverionshaveimportant significanceontheenvironmentalprotectionandresourcereclamation.Adsorption method has manyexcellences just like low-consumed, no secondarypollution and have observedeffectontheseparationoftraceamountsilverions,whichcomparedto conventionalmethod.Buttheadsorptionmethodstillhasmanyproblems,justlikethe difficultyofsorbingmaterialpreparation,highpricedandlowreusability.So,itwas badlyinneedofnewmaterialpreparation,whichhavesimplemethodtoprepared,low priced and high reusability.Thisarticlewasdirectedtothoseproblems,silverionimprintedchitosan hydrogelbeads(Ag-ICHB)andsilverionimprintedchitosangelbeads(Ag-ICGB)were prepared using Ag(Ⅰ) as template, chitosan hydrogel beads as functionalmaterials. Researchedinto theeffect ofchitosan(CTS)quantity,Ag(Ⅰ)quantity, concentrationofcoagulatingbath,temperatureofcoagulatingbath,concentrationof eluantandelutiontimeonthemasslossrate,moisturecontentandadsorptioncapacityofAg-ICHB.Studiedtheeffectofchitosanquantity,Ag(Ⅰ)quantity,concentrationofcoagulatingbath,temperatureofcoagulatingbath,temperatureofheattreatment, concentrationofeluantandelutiontimeon theswelling rateandadsorptioncapacityof Ag-ICGB.TheresearchshowsthattheAg-ICHBwouldhavehigheradsorptioncapacity, lowermasslossrateandlowermoisturecontentwhentheconcentrationofchitosanwas2.0%,CTS:Ag(Ⅰ)was1:0.1,theconcentrationofcoagulationwas22%,thetemperatureofcoagulationwas90℃,theconcentrationofeluantwas6.0g/Landthe elution time were 2h. The Ag-ICGB would have lower swelling rate and higherIIIadsorptioncapacitywhentheconcentrationofchitosanwas2.0%,CTS:Ag(Ⅰ)was1:0.1,theconcentrationofcoagulationwas22%,thetemperatureofcoagulationwas room temperature, the heat treatment temperature was 60℃, the concentration ofeluantwas8.0g/Landtheelutiontimewere4h.SpectrumofFI-IRshowsthatbonding areformedbetw