催化剂中银的含量40.docVIP

EXHIBIT 1 TO ANNEX B图示1附件B SILVER ANALYSIS银分析 SD ANALYTICAL METHOD T5分析方法- SD (Revision 2) (修订2) EXTRACTABLE SILVER IN ALUMINA SUPPORTED CATALYST BY NITRIC EXTRACTION AND SODIUM CHLORIDE TITRATION银催化剂在氧化铝支持施氮的提取和氯化钠滴定法SUMMARY概要a final weight.An aliquot is taken and analyzed for the extracted sliver using an automatic titrator equipped with a silver indicator eletrode and a doubt junction reference electrode.Standard 0.1N sodium chloride solution is the titrant. 大约50克的催化剂颗粒在150一个小时干燥后的样品硝酸溶液。冷却后稀释到。银指示电极自动滴定仪0.1 N氯化钠标准溶液。SCOPE AND APPLICATION范围和应用This method determines the amount of extractable silver in catalyst pellets.Non-extractables such as silver chloride are not recovered. It is assumed that a representative sample is in hand before the analysis is performed. 这种方法测定催化剂颗粒里可提取的银。。。SAFETY NOTES安全注Nitric acid and its solutions are very corrosive.Always wear safety glasses,acid-proof gloves and lab coat when handling. Do not breathe silver dust.Wear a dust mask or work in a hood.硝酸及腐蚀。安全眼镜、耐酸手套和实验。不银色尘埃戴防尘面罩或。MODIFICATIONS修APPARATUS AND CHEMICALS仪器Erlenmeyer flasks,1 liter,Pyrex,graduated,with 24/40. 锥型瓶,一24/40。Balance,4000g capacity readable to 0.01g,such as AND Electronic Balance Model FX-4000 or equivalent. 天平，称重4000克0.01克,如电子天平模型和FX - 4000或。Analytical balance,weighing to 0.1 mg. 分析天平,0.1毫克。Magnetic stirrer bars. 磁力搅拌子。 Graduated cylinder,200 ml.合格的圆筒，200毫升。 Volumetric pipet,25 ml. 移液管，25毫升。 Beaker,100 ml,250 ml. 烧杯100毫升250毫升。 Automatic titrator,such as Brinkmann Titrino Model 702 or equivalent,equipped with a 20 ml burette. 自动滴定仪如702型20毫升。Sliver electrode. 银电极。 Double junction reference electrode. 双盐桥参比电极。 Bottles,1 liter capacity.容量瓶，1L。 Dessicator. 干燥器。 Magnetic stirrer/hot plate. 磁力搅拌器/电热板。 Deionized water. 去离子水。 Concentrated nitric acid,ACS grade. 浓硝酸。 Sodium chloride,ACS grade. 氯化钠Sliver shot,99.99%,cat # 12186,Alfa/Johnson Matthey,P.O.Box 8247,Ward Hill,MA 1835-0747. 银99.99% 1.18Jars,with screw-on lid,4 or cap. 广口瓶，带4旋帽。 Drying oven. 烘箱。 Water condenser