己二酸二酰肼合成实验分析及过程模拟-experimental analysis and process simulation of adipic dihydrazide synthesis.docx

asrawmaterialismoresuitforindustrialproductionofADH.Keywords:adipicdihydrazide,dimethyladipate,esterification,hydrazide,Aspensimulation目录第一章文献综述..............................................................................11.1己二酸二酰肼简介..............................................................11.2合成方法..............................................................................11.2.1一步法.........................................................................11.2.2两步法.........................................................................11.2.2.1酯化反应.............................................................21.2.2.2酰肼化反应.........................................................31.2.3小结.............................................................................41.3己二酸二酰肼的应用.............................................................41.3.1在医药学方面的应用..................................................51.3.2在水性树脂方面的应用..............................................51.3.2.1水性涂料...........................................................71.3.2.2油墨....................................................................81.3.2.3胶黏剂................................................................91.4.5小结............................................................................111.5本文选题目的及研究内容...................................................12第二章己二酸二酰肼合成的实验研究............................................132.1实验部分.............................................................................132.1.1实验原理....................................................................132.1.2实验装置....................................................................142.1.3实验药品....................................................................142.1.4实验过程....................................................................142.1.5分析方法....................................................................152.2结果与讨论.........................................................................172.2.1酯化反应.............