秸秆-污泥吸附剂的制备及其特性分析-preparation and characteristics analysis of straw - sludge adsorbent.docxVIP

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秸秆-污泥吸附剂的制备及其特性分析-preparation and characteristics analysis of straw - sludge adsorbent.docx

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秸秆-污泥吸附剂的制备及其特性分析-preparation and characteristics analysis of straw - sludge adsorbent

AbstractAlong with the environmental problem getting acute in our country and people’s increasing awareness of protecting environment, the adsorbent used for the treatment of sewage and waste gas purification is increased. As a cheap, readily available and certain carbon content waste, municipal sludge and straw can be used as adsorbent materials preparation. This subject was to utilize municipal sludge and corn straw as raw materials for the preparation of the adsorbent by chemical activation. And the adsorbent prepared was used to treat the leachate for adsorption purpose.The optimum technological conditions of preparing adsorbent were studied by using a orthogonal matrix experimental method. The results showed that the prepared adsorbent was with good effect when ZnCl2 was used as an activator, and the carbonization wasconducted under a temperature of 600 ℃ for 1.5 hours with a impregnation ratio of 1:4. Inthis case, the iodine adsorption value of the adsorbent was 426.4 mg/g, and the surface area of BET was 546.5m2/g. Besides, the pore size mainly ranged from 2nm to 50 nm, mainly in hole, and the average pore size was 4.71 nm with a pore volume of 0.64 cm3/g.After our range analysis and variance analysis, four factors influencing the experimental results are listed according to the importance as follows: activatorimpregnation ratiocarbonization timecarbonization temperature.Analysis of TG/DTA and FTIR for the best adsorbent was carried out, which was mainly for the study of the adsorbent surface structure and thermodynamic characteristics. Carbonization process of raw materials mainly includes evaporation stage of water and organic matters, and then activation stage.The adsorption experiments of leachate were carried out with the best adsorption agent, and the results showed that the method could effectively remove the color and COD of leachate. After studying the adsorption conditions, we found that the best value for dosage ratio, adsorption time and pH was 3