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concentrated inverse eulsion polymerization学术英语论文.docx

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concentrated inverse eulsion polymerization学术英语论文

AbstractUsing butyl methacrylates(BMA) as monomer, Span80 as emulsifier, divinyl benzene (DVB) as cross-link agent, ammonium persulfate(APS)/sodium hydrogensulfite(SHS) as redox initiator, the high oil-absorption resin was synthesized by concentrated inverse emulsion polymerization. And the effects of different polymerization technological parameters, such as initiator, crosslinker, emulsifier, on the oil absorbency of high oil-absorption resins were discussed in detail. The result indicated that the absorption of the resin was about 9.2(g/g) for toluene and 16.2(g/g) for chloroform.Key words: concentrated inverse emulsion polymerization；oil absorption resin；oil absorption rate摘要以甲基丙烯酸正丁酯为单体，二乙烯基苯为交联剂，Span80为乳化剂，过硫酸铵/亚硫酸氢钠为氧化还原引发剂，采用超浓反相乳液法合成了高吸油性树脂。研究了引发剂用量，交联剂用量，乳化剂用量对树脂吸油性能的影响。所制备的树脂可以吸收自身重9.2倍的甲苯、16.2倍的三氯甲烷。关键字：超浓反相乳液聚合；吸油性树脂；吸油速率ContentsAbstractⅰAbstract in Chineseⅱ1 Introduction12 Experiment32.1 Materials32.2 Polymerization32.3 Measurements32.3.1 Oil absorption test32.3.2 Regeneration test42.3.3 Oil retention42.3.4 Characterization43 Results and Discussion53.1 The effect of cross-linking amount on the oil absorbency53.2 Effect of the amount of the emulsifier on the oil absorbency53.3 The effect of initiator amount on the oil absorbency63.4 Oil absorption rate of the resins73.5 Relation of oil retention ratio with time83.6 Oil absorption repetitive characteristic of resins84 Conclusions10Bibliography111 IntroductionOil pollution of marine environments is becoming a serious issue. With the growth of the off-shore petroleum industry and the necessity of marine oil transportation. Various methods for the treatment of spilled oil have been tried[1–5]. One of the methods to solve this problem is by using oil absorptive resins, which can collect and remove the oil spilled on water, and some have proved to be highly efficient[6-7]. High oil-absorption resin, being different from traditional oil-absorbing materials, is a new kind of self-swelling oil-absorbing mater